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GCMS reference standard results, DEP Labs, Feb 2002

Machine-extracted title · confidence 100%

Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations on February 25, 2002.

NYC-WTC_000009937–000009940

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

•, Data File : C:\MSDCHEM\l\5973N\02FEB21\0221C40 .D Vial: 2 Acq On : 21 Feb 2002 9:35 am Operator: Sample : cal 40 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 21 14:02:49 2002 Quant Results File: HP020702.RES

Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Last Update : Thu Feb 21 14:00:40 2002 Response via : Initial Calibration DataAcq Meth : HP020702

Compound R.T. Qlon Response Cone Unit Qvalue 35) Di-n-butylphthalate 24.87 149 14229829 36.70 ug/L 99 3 6) Fluoranthene 26.25 202 12319409 34.84 ug/L 98 3 9) Pyrene 26.88 202 12813383 35.70 ug/L 96 40) Butylbenzylphthalate 29.27 149 5820946 35.50 ug/L 99 41) Benzo(a)anthracene 30.47 228 10988369 37.33 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.12 149 8477412 41.23 ug/L 98 43) Chrysene 30.60 228 10549593 36.63 ug/L 99 45) Di-n-octylphthalate 32.85 149 13135540 29.13 ug/L 100 46) Benzo(b)fluoranthene 33.48 252 10577091m 41.35 ug/L 47) Benzo(k)fluoranthene 33.55 252 11117335 38.64 ug/L 95 48) Benzo(a)pyrene 34.28 252 10611485 40.77 ug/L 96 49) Indeno(1,2,3-cd)pyrene 37.07 276 10266753 45.38 ug/L 96 50) Dibenz(a,h)anthracene 37.15 278 8009640 42.51 ug/L 97 51) Benzo(g,h,i)perylene 37.78 276 8660357 40.92 ug/L 96

(#) = qualifier out of range (m) = manual integration 0221C40.D HP022102.M Mon Feb 25 15:41:46 2002 Page 2

NYC-WTC_000009939

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NYC-WTC_000009939Source: NYC Law Department, mirrored locally

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