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GCMS reference analysis report for sample AE02713, March 4 2002

Machine-extracted title · confidence 90%

Laboratory report documenting a reference standard run for gas chromatography-mass spectrometry analysis of sample AE02713.

NYC-WTC_000010862–000010866

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\5973N\02FEB28\0205R.D Vial: 2 Acq On : 28 Feb 2002 11:20 am Operator: Sample : ref 2/5 Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 01 09:02:46 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702

Compound R.T. Qlon Response Cone Unit Qvalue 35) Di-n-butylphthalate 24.85 149 1741808 4.86 ug/L 100 36) Fluoranthene 26.21 202 1536907 4.71 ug/L 96 3 9) Pyrene 26.84 202 1642344 4.91 ug/L 95 40) Butylbenzylphthalate 29.25 149 403621 2.64 ug/L 96 41) Benzo(a)anthracene 30.44 228 1091619 3.98 ug/L 98 42) Bis(2-ethylhexyl)phthalate 31.11 149 549525 2.87 ug/L 98 43) Chrysene 30.56 228 1329250 4.95 ug/L 98 45) Di-n-octylphthalate 32.83 149 491937 6.10 ug/L 99 4 6) Benzo(b)fluoranthene 33.45 252 794133m 3.69 ug/L 4 7) Benzo(k)fluoranthene 33.50 252 1342490 5.54 ug/L 95 48) Benzo(a)pyrene 34.25 252 638392 2.91 ug/L 96 49) Indeno(l,2,3-cd)pyrene 37.01 276 584517m 3.07 ug/L 50) Dibenz(a,h)anthracene 37.10 278 493445 3.11 ug/L 97 51) Benzo(g,h,i)perylene 37.71 276 642676 3.61 ug/L 97

(#) = qualifier out of range (m) = manual integration 0205R.D HP022102.M Fri Mar 01 09:53:35 2002 Page 2

NYC-WTC_000010865

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NYC-WTC_000010865Source: NYC Law Department, mirrored locally

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