GCMS reference standard results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

♦ 'Data File : C:\MSDCHEM\1\5973N\02FEB21\0221 Acq On : 21 Feb 2002 9:35 am (0)pVial: Operator: 2

Sample : cal 40 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 21 14:02:49 2002 Quant Results File: HP020702.RES Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Last Update : Thu Feb 21 14:00:40 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1577467 20.00 ug/L 0.00 10) Naphthalene-d8 13.21 136 7097272 20.00 ug/L 0.00 17) Acenaphthene-d10 18.34 164 3607655 20.00 ug/L 0.00 29) Phenanthrene-diO 22.64 188 5997752 20.00 ug/L 0.00 38) Chrysene-dl2 30.51 240 4884601 20.00 ug/L -0.01 44) Perylene-dl2 34.43 264 3828663 20.00 ug/L -0.02

System Monitoring Compounds 37) 2,4-DDD 27.72 235 15128 0.15 ug/L 0.00 Spiked Amount 5.000 Recovery = 3.00% Target Compounds 16 $3 Qvalue 2) n-Nitrosodimethylamine 3.99 74 3362439 43.48 ug/L 100 3) bis(2-Chloroethyl)ether 9.24 93 5063130 49.10 ug/L 99 4) 1,3-Dichlorobenzene 9.62 146 4459651 38.01 ug/L 100 5) 1,4-Dichlorobenzene 9.76 146 4440363 38.06 ug/L 99 6) 1,2-Dichlorobenzene 10.24 146 4308828 41.43 ug/L 99 7) 2,2'-oxybis (1-Chloropropa 10.68 45 7546982 46.08 ug/L 99 8) n-Nitroso-di-n-propylamine 11.06 70 3157364 41.04 ug/L 100 9) Hexachloroethane 11.04 117 1590597 39.43 ug/L 100 11) Nitrobenzene 11.37 77 4508650 36.13 ug/L 98 12) 1sophorone 12.02 82 8825992 36.84 ug/L 99 13) bis(2-Chloroethoxy)methane 12.78 93 6130819 39.17 ug/L 99 14) 1,2,4-Trichlorobenzene 13.13 180 3396935 36.98 ug/L 99 15) Naphthalene 13.26 128 12562560 35.80 ug/L 100 16) Hexachlorobutadiene 13.85 225 1643635 36.66 ug/L 98 18) Hexachlorocyclopentadiene 15.96 237 1035890 36.34 ug/L 100 19) 2-Chloronaphthalene 16.66 162 7134317 37.00 ug/L 99 20) Dimethylphthalate 17.91 163 7911688 36.15 ug/L 100 21) 2,6-Dinitrotoluene 18.09 165 1585431 31.37 ug/L 98 2 2) Acenaphthylene 17.88 152 10429691 35.34 ug/L 99 2 3) Acenaphthene 18.44 153 7124138 36.59 ug/L 99 24) 2,4-Dinitrotoluene 19.21 165 2059003 29.51 ug/L 98 25) Diethylphthalate 20.01 149 7217579 35.43 ug/L 98 26) 4-Chlorophenyl-phenylether 20.05 204 3318840 36.03 ug/L 93 27) Fluorene 19.93 166 7985831 34.01 ug/L 99 2 8) Azobenzene/1,2-Diphenylhyd 20.49 77 10417300 38.78 ug/L 97 30) N-nitrosodiphenylamine 20.45 169 4547537 29.64 ug/L 100 31) 4-Bromophenyl-phenylether 21.46 248 2168983 35.83 ug/L 98 32) Hexachlorobenzene 21.80 284 2278843 36.13 ug/L 98 33) Phenanthrene 22.72 178 11484105 34.29 ug/L 99 3 4) Anthracene 22.86 178 11748231 34.80 ug/L 100 (#) = qualifier out of range (m) = manual integration 0221C40.D HP022102.M Mon Feb 25 15:41:46 2002 Page 1

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