Laboratory data sheet for sample AE02713 analysis

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) r. Data File : C:\MSDCHEM\1\5973N\02FEB28\0228 Acq On : 28 Feb 2002 9:33 am 6od Vial: Operator: 2 Sample : cal 40 Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 01 09:54:07 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1439437 20.00 ug/L 0.00 10) Naphthalene-d8 13.21 136 6420208 20.00 ug/L 0.00 17) Acenaphthene-diO 18.34 164 3292091 20.00 ug/L 0.00 2 9) Phenanthrene-dl0 22.64 188 5508700 20.00 ug/L 0.00 38) Chrysene-dl2 30.51 240 4401042 20.00 ug/L -0.01 44) Perylene-dl2 34.43 264 3409139 20.00 ug/L -0.02 System Monitoring Compounds 37) 2,4-DDD 27.72 235 15349 0.21 ug/L 0.00 Spiked Amount 5.000 Recovery = 4.20% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.98 74 2911078 41.26 ug/L 98 3) bis(2-Chloroethyl)ether 9.24 93 4506867 47.90 ug/L 99 4) 1,3-Dichlorobenzene 9.61 146 4072283 38.04 ug/L 98 5) 1,4-Dichlorobenzene 9.76 146 4046258 38.01 ug/L 99 6) 1,2-Dichlorobenzene 10.24 146 3948877 41.61 ug/L 100 7) 2,2'-oxybi s (1-Chloropropa 10.68 45 6739512 45.10 ug/L 99 8) n-Nitroso-di-n-propylamine 11.06 70 2848789 40.58 ug/L 100 9) Hexachloroethane 11.03 117 1447243 39.31 ug/L 96 11) Nitrobenzene 11.37 77 4133778 36.62 ug/L 99 12) 1sophorone 12.02 82 8014486 36.98 ug/L 99 13) bis(2-Chloroethoxy)methane 12.78 93 5488647 38.77 ug/L 99 14) 1,2,4-Trichlorobenzene 13.13 180 3098819 37.29 ug/L 98 15) Naphthalene 13.26 128 11333207 35.70 ug/L 100 16) Hexachlorobutadiene 13.85 225 1525764 37.62 ug/L 99 18) Hexachlorocyclopentadiene 15.96 237 1169580 44.96 ug/L 98 19) 2-Chioronaphthalene 16.66 162 6525046 37.08 ug/L 99 20) Dimethylphthalate 17.91 163 7328100 36.69 ug/L 99 21) 2,6-Dinitrotoluene 18.09 165 1591966 34.52 ug/L 96 22) Acenaphthylene 17.88 152 9576472 35.56 ug/L 100 2 3) Acenaphthene 18.44 153 6463166 36.38 ug/L 98 24) 2,4-Dinitrotoluene 19.20 165 2088175 32.79 ug/L 90 25) Diethylphthalate 20.01 149 6649830 35.77 ug/L 99 26) 4-Chlorophenyl-phenylether 20.05 204 3135330 37.30 ug/L 92 27) Fluorene 19.93 166 7473854 34.88 ug/L 100 2 8) Azobenzene/1,2-Diphenylhyd 20.49 77 9434664 38.49 ug/L 98 30) N-nitrosodiphenylamine 20.45 169 4159154 29.52 ug/L 99 31) 4-Bromophenyl-phenylether 21.45 248 2027758 36.47 ug/L 95 32) Hexachlorobenzene 21.80 284 2186721 37.74 ug/L 95 3 3) Phenanthrene 22.72 178 10604410 34.47 ug/L 100 34) Anthracene 22.86 178 10894235 35.14 ug/L 100 (#) = qualifier out of range (m) = manual integration 0228C40.D HP022102.M Fri Mar 01 09:55:09 2002 Page 1

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