Calibration table page listing internal standards and response factors for GCMS analysis.
NYC-WTC_000009650–000009656Folder label: “GCMS X 1/14/02 A 3/4/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\FEB1502\1143.D Vial: 5 Acq On : 15 Feb 2002 7:23 pm Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 4 15:03 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) t Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 457715 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 1720621 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.29 164 944160 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.74 188 1318897 20.00 ug/1 -0.03 38) Chrysene-dl2 33.81 240 892492 20.00 ug/1 -0.04 44) Perylene-dl2 38.09 264 603463 20.00 ug/1 -0.04
System Monitoring Compounds 37) 2,4-DDD 30.81 235 50373 3.66 ug/mL 0.32 Spiked Amount 5.000 Recovery = 73.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 1268 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.76 149 357 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 23.37 166 355 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1143.D GCMS0208.M Mon Mar 04 15:04:04 2002 Page 1
NYC-WTC_000009650
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Laboratory file showing GC/MS calibration response factors for surrogate compounds from February and March 2002.
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Laboratory file showing GC/MS calibration response factors for surrogate compounds from February and March 2002.
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Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
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