GCMS calibration table with surrogate recovery data, Feb 16, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1502\1137.D Vial: 10 Acq On : 16 Feb 2002 12:12 am Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 4 15:01 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table .' p Last Update : Wed Feb 27 11:30:15 2002 AP Response via : Initial Calibration 1 DataAcq Meth : GCMS0208 CN l

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 438597 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 1676800 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 900901 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.74 188 1283057 20.00 ug/1 -0.02 38) Chrysene-dl2 33.81 240 909628 20.00 ug/1 -0.03 44) Perylene-dl2 38.09 264 654677 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 30.81 235 55882 4.17 ug/mL 0.31 Spiked Amount 5.000 Recovery = 83.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichiorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 799 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 381 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1137.D GCMS0208.M Mon Mar 04 15:02:18 2002 Page 1

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