NYC-WTC_000006371
Initial GCMS analysis report for sample AE01940 conducted by analyst DLV on March 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 6 pages
GCMS calibration table for deuterated compounds, Feb 2002
Machine-extracted title · confidence 100%Calibration table listing retention times and responses for deuterated standards including naphthalene-d8.
NYC-WTC_000006387–000006392Folder label: “GCMS X 2/15/02 A 2/9/02 & 2/16/02”
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NYC 9/11 Public Portal Document V tcii —
Data File C:\HPCHEM\l\DATA\FEB0802\1941.D Vial: 21 Acq On 9 Feb 2002 4:46 am Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 8:44 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.34 152 299572 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1139055 20.00 ug/1 0.00 17) Acenaphthene-dlO 21.30 164 611799 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 870060 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 555722 20.00 ug/1 -0.02 44) Perylene-dl2 38.10 264 353823 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.83 235 35934 3.32 ug/mL 0.34 Spiked Amount 5.000 Recovery = 66.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) his(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 557 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 211 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1941.D GCMS0208.M Fri Mar 08 15:30:00 2002 Page 1
NYC-WTC_000006387
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