GCMS analysis results for sample AE03251, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document ulDlaly searcn Lopoura Keporc

Data File : C:\MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 ■ Acq On : 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Propenamide $$ Acrylamide... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.65 0.08 ug/L 33577 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenamide $$ Acrylamide $$ E... 71 C3H5NO 000079-06-1 4 2 Furan, 2,5-dihydro-3-methyl- (CA... 84 C5H80 001708-31-2 4 3 N-Methyl-7-azabicyclo(2,2,1)hept... 109 C7H11N 000000-00-0 4 4 2,7-OCTADIENE, 1-METHOXY- $$ 1-M... 140 C9H160 014543-49-8 2 Abundance Scan 113 (4.649 min): 03251.0 (-) m/z 41.10 100.00% 41 71 57 88 5000

51 n y ! A , aA ! ) y m/z-> O+ 1" i"" i'" ' i"■ ■ i" "i L i" " r " ■ i " ■ i" " i" " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 ' i" ‘11" ‘' i" " i" " i"" i ■" m/z 4.40 71.00 4.60 4.80 5.00 89.55% Abundance #1430:2-Propenamide $$ Acrylamide $$ Ethylenecarboxamide... 71

5000 27 44 55 -.. AA.... .. 4.40 4.60 4.80 5.00 m/z 57.00 67.40% O+ 1" ।।" I" " । I! I I I I I I I I i1" 1 r 1" I —TTTTTTTT i"111 ’"11" " i" " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #3355: Furan, 2,5-dihydro-3-methyl- (CAS) $$ 3-METHYL-2.5-... 41 84 69 4.40 4.60 4.80 5.00 5000 56 m/z 88.00 65.13%

51 0 xroagorog m m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 #11828: N-Methyl-7-azabicyclo(2,2,1)hept-2-ene 39 4.40 4.60 m 4.80 5.00 53 m/z 53.10 53.65%

5000 80 v 47 — — mm ' lip 109 0 " i" " i" " i" " i"'11"1 ‘ i"' ■ ■ i ■ ■ ■ 1 i mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 4.40 4.60 4.80 5.00

)3251.D HP022102.M Mon Mar 04 12:33:47 2002 Page 6

NYC-WTC_000006215

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NYC-WTC_000006215Source: NYC Law Department, mirrored locally

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