GCMS surrogate recovery results, sample AE00162, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1402\162.D Vial: 34 Acq On : 15 Feb 2002 11:14 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************** ******** * * *** ******** * * Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.31 0.28 ug/1 29481 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual ---------------------- 7------------------------------ 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 Morpholine,/4-methyl- 101 C5H11NO 000109-02-4 9 3 2-Heptanone, 7,7-dichloro- 182 C7H12C12O 000000-00-0 9 4 2-Propanone, Abundance / 1-(1Scan -methyl ethoxy) - 356 (8.310 min): 162.D (-) 116 C6H12O2 042781-12-4 9 m/ z 43.05.....100.00% 43

5000 59 ............... 101 ‘ ■ i 1 ' 1 1 i ■ ■ 1 ■ i 1 1 ■ ■ i 8.00 8.20 8.40 8.60 36,1114* 49 TI J..........93....... 1..... m/z 59.05 44.96%

y m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyi- 43 5000 TTI 59 8.00 8.20 8.40 8.60 m/z 100.95 18.11% 15 31 i . 101 83 | -PP i ' ■ 1 ' i ' ■ 1 1 i ■ ' 1 ■ i ' ■ ■ 1 i 1 ■ ' ‘ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 43

8.00 8.20 8.40 8.60 5000 m/z 58.05 14.40% 101 15 71 27 56 ' ■ i ' ' ' ■ i ' ' ' ' i ' ' ' ' i ’ 1 ' ' i ' ' i ' ' ' ' i ' 1 I ' ' 1 ‘ I ' 1 ' ' I ' 1 1 ' I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #18211: 2-Heptanone, 7,7-dichloro- 43 8.00 8.20 8.40 8.60 58 m/ Z 41.05 7.63% 5000

53 67 , 75 1 03 m/z-> ... 10 20 npo 30 38,1 40 ■ ■ I ■ 50 ■ 60 70 80 90 100 110 8.00 8.20 8.40 8.60

162 .D GCMS0208.M Fri Feb 15 14:01:13 2002 Page 1

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