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GCMS analysis results for sample AE02966, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02966 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005627–000005641

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

I Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB0802\2966.D Vial: 30 Acq On 9 Feb 2002 1:30 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 9:58 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.82 178 199 N.D. 34) Anthracene 25.82 178 199 N.D. 35) Di-n-butylphthalate 27.72 149 2856 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.82 228 2163 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 2510 N.D. 43) Chrysene 33.90 228 617 N.D. 45) Di-n-Octylphthalate 35.78 149 172 N.D. 46) Benzo(b)fluoranthene 36.89 252 1001 N.D. 47) Benzo(k)fluoranthene 36.95 252 911 N.D. 48) Benzo(a)pyrene 37.90 252 693 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 2966.D GCMS0208.M Wed Feb 13 09:59:04 2002 Page 2

NYC-WTC_000005630

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NYC-WTC_000005630Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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