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GCMS analysis results for sample AE02972, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02972 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005679–000005688

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\FEB0802\2972.D Vial: 36 Acq On 9 Feb 2002 7:19 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 10:50 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.75 178 353 N.D. 34) Anthracene 25.75 178 353 N.D. 35) Di-n-butylphthalate 27.71 149 5117 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.90 228 5796 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 4300 N.D. 43) Chrysene 33.90 228 5951 N.D. 45) Di-n-Octylphthalate 35.77 149 2707 N.D. 46) Benzo(b)fluoranthene 36.89 252 3765 N.D. 47) Benzo(k)fluoranthene 36.95 252 10397 N.D. 48) Benzo(a)pyrene 38.12 252 2660 N.D. 49) Indeno(1,2,3-cd)pyrene 42.31 276 2847 N.D. 50) Dibenz(a,h)anthracene 42.40 278 3831 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 2972.D GCMS0208.M Wed Feb 13 10:51:01 2002 Page 2

NYC-WTC_000005682

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NYC-WTC_000005682Source: NYC Law Department, mirrored locally

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