Laboratory report for DEP sample AE02966 showing unknown compounds and surrogate recovery data from February 15, 2002.
NYC-WTC_000005627–000005641Folder label: “GCMS X 2/7/02 A 2/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\FEB0802\2966.D Vial: 30 Acq On 9 Feb 2002 1:30 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 9:58 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 338866 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1302884 20.00 ug/1 0.00 17) Acenaphthene-dlO 21.31 164 706572 20.00 ug/1 0.00 29) Phenanthrene-diO 25.75 188 1017902 20.00 ug/1 -0.01 38) .Chrysene-dl2 33.82 240 652408 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 449715 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.83 235 46416 3.67 ug/mL 0.33 Spiked Amount 5.000 Recovery = 73.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 253 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.78 149 10687 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 2966.D GCMS0208.M Wed Feb 13 09:59:00 2002 Page 1
NYC-WTC_000005629
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NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016136
GCMS analysis report for sample AD31377 showing surrogate recovery and unknown compounds from February 7, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016667
Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009773
Analytical results page for sample AE01231 processed on February 25, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035195
Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28689.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050165
Laboratory report documenting GCMS analysis of sample AE00007 with detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016125
GCMS analysis report for sample AD27392 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049745
GCMS analysis report for sample AD31641 conducted on February 11, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034971
Blank test results confirming no detectable contaminants above method detection limits for sample AD28662.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035460
GCMS scan results for sample AD28802 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and other compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037255
Gas chromatography-mass spectrometry report documenting analysis of sample AD30013 conducted on January 28, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Instrument sequence log listing sample IDs and analytical runs processed on February 8, 2002, including calibration checks.
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Laboratory report for DEP sample AE02966 listing concentrations of target compounds including nitrosamines and chlorobenzenes.
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Reference analysis report for DEP sample AE02966 showing measured values for target compounds against detection limits.
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