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GCMS analysis results for sample AE02646, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02646.

NYC-WTC_000005435–000005447

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005444
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR0702\2646.D Vial: 19 Acq On : 8 Mar 2002 7:26 am Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

18.05 0.41 ug/1 66121 Naphthalene-d8 15.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7—Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 17 2 Silane, [1,2/3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 9 3 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 9 4 2H-1,4-Be: ;odiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 7 Abundance Scan 1417 (18.050 min): 2646.D (-) m/z 73.00....100.00% 73

5000 341 147 429 45 18.00 18.20 18.40 ................ — 1110 |....... 207.... 251........ 311 —0101-01-10111131111111500111100110011100113111100011 1.... " i1H' i" " r1'1 r m/z17.80 —0010—000300703" 341.00 39.98% m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420 Abundance #56714: 1,1.1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiioxyjt 73

147 5000 267 355 429 17.80 18.00 18.20 18.40 45 207 I m/z 147.00 16.61%

m/z-> _ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance • . ’ ■ T .. 5 73

239 17.80 18.00 18.20 18.40 5000 342 m/z 342.00 14.28% 45 133 179 211 314 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 ' Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 17.80 18.00 18.20 18.40 341 m/z 325.00 12.06% 429 5000

147 | m/z-> .... 1.. J17..|..... ...... ................. . H-rp 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 L 17.80 18.00 18.20 18.40 i

2646.D GCMS0208.M Wed Mar 13 14:56:29 2002 Page 3

NYC-WTC_000005444

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NYC-WTC_000005444Source: NYC Law Department, mirrored locally

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