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GCMS blank analysis report, Feb 2002

Machine-extracted title · confidence 95%

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

NYC-WTC_000005159–000005166

Folder label: “GCMS X 2/4/02 A 2/8/02

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Scanned page image, NYC-WTC_000005163
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\FEBO 8 02\LB.D Vial: 5 Acq On 8 Feb 2002 1:11 pm Operator: 209 GALOS Sample GC/MS SCAN 2/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak. peak % of # min scan scan scan TY height area % max. total

1 8.226 344 347 357 rBV 10346 25863 1.03% 0.206% 2 12.347 790 796 812 rVB 821722 1950698 77.82% 15.501% 3 15.992 1185 1193 1209 rBV 1192603 2387054 95.23% 18.968% 4 21.307 1766 1772 1782 rBV 1248166 2506588 100.00% 19.918% 5 25.760 2250 2257 2268 rBV2 1164763 2396541 95.61% 19.044%

6 30.837 2805 2810 2817 rBV 161134 300856 12.00% 2.391% 7 33.829 3129 3136 3150 rBV 801631 1759467 70.19% 13.981% 8 38.117 3594 3603 3623 rBV2 421470 1257343 50.16% 9.991%

Sum of corrected areas: 12584410

LB.D GCMS0208.M Mon Feb 11 12:33:56 2002

NYC-WTC_000005163

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NYC-WTC_000005163Source: NYC Law Department, mirrored locally

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