DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02385.D Vial: 1 Acq On : 27 Feb 2002 3 :17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 4 1,3,5-Cycloheptatriene $$ C... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 4.38 0.11 ug/L 50459 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5-Cycloheptatriene $$ Cycloh... 92 C7H8 000544-25-2 9 2 METHYLFULVENE 92 C7H8 000000-00-0 9 3 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 9 4 N-(2-THIAZOLYL)-2-NITRO-3-BENZYL... 369 C18H15N3O4S 000000-00-0 9 Abundance Scan 89 (4.379 min): 02385. D (-) m/ z 91.10 100.00% 91

5000

,........... 43 50 55 65 85 4.00 4.20 4.40 4.60 4.80 0! ■ ■ | ' 1 ■ 1 | ■ ■ ■ ■ | ■ 1 ' 1 | 1 1 । । | । ' ( ■ | ' > 1 I | 1 I H I I ! | 1 I I . | I I I I | ! I , I | I I . I | ! 1 I I | Il I I | ■' i'''' i' 1 m/z 92.00 59.29% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5570:1,3,5-Cycloheptatriene $$ Cyclohepta-1,3,5-triene $... 91

5000 4.00 4.20 4.40 4.60 4.80 65 m/ Z 65.10 12.12% 27 m/z-> Ot TTp- 20 ---H 38

25 30 35 40 45 50 55 60 65 „6144 70 75 IIPPTITTTTTTTTTTT ’ ’’’4111 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91 . I < 1

400 4.204.40 4.60 4.80 5000 m/z 85.00 7.15%

39 65 1 45 61,1 0! 111' ■ " i'■ " i “ ‘■i11111" 111rri 1111111 > ।111111111 i1' ■ ■ i ■11' i ■ ■' ■ i ■ ■111 . .... m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 4.00 LA D. 4.20 4.40 4.60 4.80 m/z 43.10 7.13%

Tl/Z-> 5000

39 .1 65 61 , | —— 86 0 111" " i " 111 " " i1'111" " Irr " 111111" " 111'11'1111 " 111" 1111' " 11''11 20 25 30 35 40. 45 50 55 60 65 70 75 80 85 90 95 100 4.00 L 4.20 4.40 4.60 1944 1 4.80

32385.D HP022102.M Thu Feb 28 08:47:02 2002 Page 6

NYC-WTC_000005015

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999