DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Dzca File : C: \MSDCHEM\1\5973N\02FEB27\02386.D Vial: 2 Acq On : 27 Feb 2002 4:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Phthalic acid, diisooctyl e... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

31.11 0.06 ug/L 47649 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 45 2 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 45 3 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 45 4 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 38 Abundance Scan 2457 (31.111 min): 02386.D (-) m/z 149.00 100.00% 149

5000 167 57 V N.......... 43 70 1 1 1 1 1 1 ' 1 i ■ ' ' ' 1 104 236 30.80 31.00 31.20 31.40 1 84 ----- 0- T-|—t—r-r-r-[—r-r-r m/z 167.00 41.51% m/z-> 80 140 100 160 180 120200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 149

5000 ' ■ i 1 ■ ' ' 1 1 1 ' I ' ' ' ' I ' 1 ' ' I 57 167 30.80 31.00 31.20 31.40 71 m/z 57.10 29.81% 83 — 113 i 0 ....... I1 | ' 1 , .97 .1........ II, , , , ' ' 1 1 >! 1 | I I I I | I I I I | I I I । | ’

niz-> 40 60 80 100 180 200 120 220 140 160 240 Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149 30.80 31.00 31.20 31.40 5000 m/z 43.10 22.86% 57 167 71 83 113 1

mfe-> O—T 40 111187 .17.... .H 80 100 120 140 160 180 200 220 240 Abundance #326907:1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) e... 1 ' r1 1 ' [ ' 1 1 ' I 149 30.80 31.00 31.20 31.40 m/ Z 70.00 20.73%

5000 57 167 71

m/z-> 42 0' ■ 1 1 1 40 Tut 60 111.987, mmmpa 83

80 —

100 113

120 140 ,

160 1 1 1 1 180 1 ' 1 200 1 1 ■ ■ ■ 1 1 220 1 ■ ‘ 1 ‘ 240 r 30.80 31.00 31.20 31.40

02386.D HP022102.M Thu Feb 28 08:47:11 2002 Page 15

NYC-WTC_000005044

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NYC-WTC_000005044Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999