DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound. Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02386.D Vial: 2 Acq On : 27 Feb 2002 4:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 Acetic acid, 3- [1,3]dioxola... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.94 0.46 ug/L 248146 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 38 3 1-Propene-l-thiol 74 C3H6S 000925-89-3 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 227 (5.936 min): 02386.D (-) m/z 73.10 100.00% 73

5000 43 PT—m—uCOTTT 5.60 5.80 6.00 6.20 87 103 m/z-> 0- . ....... 20 Il In I'155‘ 11' ‘ —p-m-mpm 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 24.83% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7(3

5000 AATII —A 1 1 i 1 ■ ' ' I ' ' ' 1 r 5.60 5.80 6.00 6.20 43 m/z 41.10 9.92% 27 55 113 87 174 0-IjIni.......... 'I1’1' > i ■ ■ > ■ । ■ ‘I’ 11111 TTTTTTTTTTTTTITTTi1" Tr m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 A.M., 5.60 —AAA 5.80 6.00 6.20 5000 m/z 45.10 8.82% 43 27 55.......... ................................. ...................................................... 0 TTTTTTTT miz- Abundance 20 . 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 70 #2002:1-Propene-1-thiol ... A 5.60 5.80 A 6.00 6.20 m/z 71.0.0 5.39%

5000 43

m/z-> 1 O-TTTT 11' i Iln i'1 ~i'i n 11 20 30 40 50 60 70 57 ‘/ 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02386.D HP022102.M Thu Feb 28 08:47:10 2002 Page 8

NYC-WTC_000005037