GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.614 17 21 25 rW 35791 61549 0.28% 0.053% 2 4.253 73 77 83 rBV2 16499 44720 0.20% 0.038% 3 5.920 219 223 233 rBV 75395 167003 0.75% 0.143% 4 6.582 275 281 287 rVB 22302 51726 0.23% 0.044% 5 9.550 539 541 547 rBV2 16877 38137 0.17% 0.033%

6 9.710 551 555 561 rW 6875034 12810484 57.72% 10.945% 7 9.847 565 567 573 rBV 29089 80208 0.36% 0.069% 8 10.007 579 581 593 rVB2 14366 34603 0.16% 0.030% 9 13.192 855 860 865 rBV 8978455 18433255 83.06% 15.749% 10 13.375 873 876 883 rVB2 20103 44291 0.20% 0.038%

11 16.549 1151 1154 1159 rBV 25698 45408 0.20% 0.039% 12 18.341 1305 1311 1317 rBV 9534666 20334715 91.62% 17.374% 13 22.280 1651 1656 1661 rW 112452 199897 0.90% 0.171% 14 22.646 1681 1688 1693 rBV2 9249342 22193982 100.00% 18.962% 15 22.771 1695 1699 1731 rVB 149768 611596 2.76% 0.523%

16 24.849 1875 1881 1885 rVB 17471 33738 0.15% 0.029% 17 27.726 2127 2133 2139 rW 1193059 2158941 9.73% 1.845% 18 29.678 2301 2304 2309 rBV3 20676 51160 0.23% 0.044% 19 30.500 2369 2376 2381 rBV2 7956439 21520925 96.97% 18.387% 20 34.428 2713 2720 2753 rBV 6135686 18126752 81.67% 15.487%

Sum of corrected areas: 117043090

28324A.D SCAN508.M Fri Feb 22 11:44:11 2002 Page 1

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