GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.499 7 11 15 rBV 43642 65046 0.26% 0.049% 2 3.613 17 21 31 rW 54655 88839 0.36% 0.067% 3 3.922 45 48 53 rW 29595 46757 0.19% 0.036% 4 4.241 71 76 81 rW 304765 539983 2.19% 0.410% 5 5.920 219 223 229 rBV 94679 197392 0.80% 0.150%

6 6.011 229 231 235 rW 24051 41741 0.17% 0.032% 7 6.582 277 281 287 rBV 25537 45874 0.19% 0.035% 8 9.710 551 555 561 rW 7602767 15042853 60.99% 11.422% 9 9.847 561 567 573 rVB 18276 48769 0.20% 0.037% 10 10.007 579 581 587 rVB 32402 52261 0.21% 0.040%

11 13.204 855 861 865 rBV 9886257 21520260 87.25% 16.341% 12 13.375 871 876 881 rVB 24808 48532 0.20% 0.037% 13 16.549 1151 1154 1157 rVB 28573 53458 0.22% 0.041% 14 18.341 1305 1311 1317 rBV 10372794 23203389 94.08% 17.619% 15 22.280 1651 1656 1661 rBV 121097 226030 0.92% 0.172%

16 22.645 1681 1688 1693 rBV2 9798012 24664318 100.00% 18.728% 17 22.771 1697 1699 1719 rVB 164945 486649 1.97% 0.370% 18 27.726 2129 2133 2139 rBV 1439393 2568618 10.41% 1.950% 19 30.512 2369 2377 2381 rBV 8209059 23059528 93.49% 17.509% 20 34.428 2713 2720 2765 rBV 6555534 19697327 79.86% 14.956%

Sum of corrected areas: 131697624

29232A.D SCAN508.M Fri Feb 22 11:44:17 2002 Page 1

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