GCMS analysis results for sample AD29522, Feb 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D Vial: 4 Acq On 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 f Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 19 21 25 rBV 33342 53348 0.39% 0.073% 2 3.922 45 48 53 rBV 17601 29463 0.22% 0.040% 3 5.920 221 223 239 rBV 78979 195775 1.44% 0.268% 4 9.710 551 555 561 rW 4343769 8487382 62.58% 11.615% 5 9.858 561 568 575 rVB 14104 30865 6.23% 0.042%

6 12.541 799 803 807 rW 41045 67119 0.49% 0.092% 7 13.192 855 860 865 rBV 6260394 11976265 88.31% 16.390% 8 13.375 873 876 881 rVB2 13983 26241 0.19% 0.036% 9 15.624 1067 1073 1077 rBV2 14226 27364 0.20% 0.037% 10 16.549 1151 1154 1159 rVB2 15266 31444 0.23% 0.043%

11 18.341 1305 1311 1315 rBV 6390280 12843050 94.70% 17.576% 12 19.974 1451 1454 1465 rW3 10575 24655 0.18% 0.034% 13 22.280 1653 1656 1661 rW2 50316 98020 0.72% 0.134% 14 22.634 1681 1687 1693 rBV2 5769957 13562220 100.00% 18.560% 15 22.771 1697 1699 1705 rVB 79935 161468 1.19% 0.221%

16 27.726 2129 2133 2139 rBV 893435 1596218 11.77% 2.184% 17 29.496 2283 2288 2295 rBV3 15868 38889 0.29% 0.053% 18 30.489 2369 2375 2411 rBV 5099453 13117119 96.72% 17.951% 19 31.094 2425 2428 2435 rW 13029 36925 0.27% 0.051% 20 34.416 2713 2719 2757 rBV 3953781 10668393 78.66% 14.600%

Sum of corrected areas: 73072223

29522.D SCANS08.M Mon Feb 04 08:41:10 2002 Page 1

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