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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004238
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

36.50 0.63 ug/1 265680 Perylene-dl2 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Isopropoxy-1/, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 1,2-Benzenedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 37 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 23 Abundance 1' Scan 3426 (36.499 min): 30651 .D (-) " m/ z 73.00 100.00% 73

147 5000 221 281 geg 36.20 36.40 36.60 36.80

m/z~> 45 TTTT 50 117 100 —19— 250 150 .3271 401429 200300 350 400 450 500 550 m/z 147.00 51.53% Abundance #60503: 3-lsoprapoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

r P// P TT 5000 147 36.20 36.40 36.60 36.80 m/z " 34.43% 221 281 327 -i 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 72072. 1 2-Benzenedicarboxylic acid, bisttrimethylsily!) e 147 FTIImmmTT1" ■ f' ' 73 36.20 36.40 36.60 36.80 5000 m/ Z 281.00 18.76% 45 295 119 | 193 221 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester I 73 36.20 36.40 36.60 36.80 m/z 207.00 15.84%

AA 147 5000

45

miz-> ‘I" ' 50 100 117 150 29 200 250 300 350 400 450 500 550 36.20 36.40 36.60 36.80

30651.D GCMS1126.M Mon Jan 28 12:24:20 2002 Page 18

NYC-WTC_000004238

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NYC-WTC_000004238Source: NYC Law Department, mirrored locally

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