DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\30704.D Vial: 1 Acq On : 1 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 8 Cyclooctane-dl6 (CAS) Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

18.73 0.11 ug/L 64638 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclooctane-dl6 (CAS) 128 C8D16 092204-03-0 5 tO | 2 4-Acetyl-3-methylpyrazole Amidin... 180 C7H12N6 093584-04-4 5 3 Benzene, l-chloro-4-(trifluoroet... 192 C8H4C1F3 082907-01-5 5 4 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 5 Weloy Abundance Scan 1345 (18.729 min): 30704.D (-) m/z 64.00 100.00% 64

192

5000- 128 162

N 86 96 180 18.40 18.60 18.80 19.00 0 i ■ ■ ■ ‘ । "11 ■ ■111 ■ ■ i1" 11" 1111tt[11 I I I I I ■ > [ I > i1' " i1" 11 ■1 " i1 ■ I... rrpi rq rr m/z 191.80 64.46% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #14058: Cyclooctane-d16 (CAS) 43 64

5000 30 80 94 18.40 18.60 18.80 19.00 128 m/z 127.90 26.56% 0 11, 1 * ।11 TTTT i " " i11" i1 " ■ r ■" i " “ i " " i " m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #85649: 4-Acetyl-3-methylpyrazoIe Amidinohydrazone $$ 5-Ac... 64 ....... । ■ ■ 1 ■ i ■ ' 1 ' 1 1 ’ I 18.40 18.60 18.80 19.00 5000 m/z 162.10 23.20% 108 124 165 22000000 180 0 ‘111211111111111111 " i " " i" " i" ■ ■ r' ■ i" “ r 1’1**11111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102085: Benzene, 1-chloro-4-(trifluoroethenyl)- (CAS) 19/2 18.40 18.60 18.80 19.00 m/z 66.00 18.82% 107 157 5000 137

0 " ' i" ‘11" " i " " i " " r ‘ " I " " i " " i " “ i'1" r ' " i " " i'" 11 ■ ■ " i " " i" " i " " i " i ■1 / y............ .............. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.40 18.60 18.80 19.00

30704.D SCAN508.M Mon Feb 04 08:41:25 2002 Page 10

NYC-WTC_000004122

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NYC-WTC_000004122Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999