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GCMS analysis results for sample AE01464, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01464 conducted on March 6, 2002.

NYC-WTC_000003607–000003617

Folder label: “GCMS X 1/23/02 A 2/22/02

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Scanned page image, NYC-WTC_000003612
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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\l\DATA\FEB2102\1464.D Vial: 19 Acq On : 22 Feb 2002 9:47 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.950 749 752 757 rBV 11230 23228 1.29% 0.262% 2 12.033 757 761 767 rVB 11260 25427 1.41% 0.287% 3 12.253 781 785 788 rBV 17621 39233 2.17% 0.443% 4 12.326 788 793 806 rVB 501236 1281551 71.03% 14.458% 5 15.971 1184 1190 1204 rBV 816245 1665949 92.33% 18.795%

6 21.286 1763 1769 1783 rBV 893166 1804346 100.00% 20.356% 7 25.730 2247 2253 2265 rBV2 755369 1643034 91.06% 18.536% 8 27.694 2463 2467 2474 rVB 13871 25108 1.39% 0.283% 9 30.815 2801 2807 2815 rVB 111797 222457 12.33% 2.510% 10 33.799 3125 3132 3150 rBV2 532655 1207588 66.93% 13.624%

11 38.077 3590 3598 3616 rBV2 305790 925893 51.31% 10.446%

Sum of corrected areas: 8863814

1464.D GCMS0208.M Tue Feb 26 15:05:48 2002

NYC-WTC_000003612

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NYC-WTC_000003612Source: NYC Law Department, mirrored locally

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