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GCMS analysis results for sample AD31592, Feb 28 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31592 conducted on February 28, 2002.

NYC-WTC_000038220–000038233

Folder label: “GCMS X 2/21/02 A 2/22/02

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Scanned page image, NYC-WTC_000038225
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

t LSC Area Percent Report • Data File : C:\HPCHEM\l\DATA\FEB2102\31592.D Vial: 42 Acq On : 23 Feb 2002 7:32 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.204 339 344 37C rVB 79826 257918 14.27% 2.746% 2 12.326 788 793 810 rVB 478147 1303644 72.11% 13.881% 3 15.970 1184 1190 1206 rBV 808832 1715806 94.91% 18.270% 4 21.286 1763 1769 1781 rBV 897594 1807876 100.00% 19.250% 5 25.729 2247 2253 2265 rBV2 778008 1711739 94.68% 18.227%

6 30.815 2802 2807 2813 rVB 102324 204416 11.31% 2.177% 7 33.798 3126 3132 3151 rBV2 574569 1332538 73.71% 14.189% 8 34.010 3151 3155 3162 rVB2 7306 18545 1.03% 0.197% 9 36.277 3397 3402 3409 rBV3 6288 18260 1.01% 0.194% 10 38.086 3591 3599 3615 rBV2 318040 1020680 56.46% 10.868%

Sum of corrected areas: 9391422

31592.D GCMS0208.M Wed Feb 27 12:07:09 2002

NYC-WTC_000038225

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NYC-WTC_000038225Source: NYC Law Department, mirrored locally

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