GCMS analysis results for sample AE01140, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01140 -D Vial: 6 . Acq On : 25 Feb 2002 3:22 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Ethanol, 2,2-dichloro- $$ D... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.78 0.09 ug/L 35395 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2,2-dichloro- $$ Dichlo... 114 C2H4C120 000598-38-9 2 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 2 3 ISOCYANIC ACID $$ Carbimide $$ H... 43 CHNO 000075-13-8 2 4 2-Pentanone, 3-ethyl- 114 C7H140 006137-03-7 2 Abundance Scan 36 (3.780 min): 01140.D (-) m/z 43.10 100.00% 43

5000

n | A,/——/ 51 63 83 3.60 3.80 4.00 4.20 11 + Of । i li 1 r11 1 1 1 11 1 1 1 1 1 1 ■ i ■ ' ' ■ । 1 ■ ■ 1 i ■ ■ ■ ■ i ■ ‘ ■ i ■ ■ ' ‘ i ■ m/z 83.00 6.57% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #14465: Ethanol, 2,2-dichloro- $$ Dichloroethanol $$ 2,2-D... 3

5000 3.60 3.80 4.00 4.20 m/z 63.00 5.20% 43 49 61 83 114 01 1 1 i ' ' ' ' i ' ' ' ' i ' 1 — T1——PTTTITTIPTTPPT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #21994: 2-Propanone, 1,1-dichloro- 43 * 3.60 3.80 4.00 4.20 5000 m/z 42.10 4.68%

27 — 49 63 83 91 126 I 36 0+ TIPP miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #181: ISOCYANIC ACID $$ Carbimide $$ Hydrogen isocyanate 43 3.60 3.80 4.00 4.20 m/z 47.00 4.53%

5000

15

m/z—> 0 1111.7 10 20 30 40 1 ■ 1 i ■ ' 1 FFi । । । । 50 60 70 80 । । । . . . > । . . . . । 90 100 110 । । 120 । । । । . 130 3.60 3.80 4.00 4.20

01140.D HP022102.M Tue Feb 26 08:30:17 2002 Page 5

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