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GCMS results for sample AE00702, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051895–000051913

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

*— X ‘ L

Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 . Acq On : 16 Jan 2002 3:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************************************** * * **** * * * * Peak Number 4 Ethanol, 2-butoxy- (CAS) $$. .. Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 7.43 0.72 ug/L 263856 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2-butoxy- (CAS) $$ 2-Bu... 118 C6H1402 000111-76-2 86 2 Ethanol, 2-butoxy- (CAS) $$ 2-Bu... 118 C6H14O2 000111-76-2 83 3 Ethanol, 2-butoxy- $$ .beta.-But... 118 C6H14O2 000111-76-2 83 4 Ethanol, 2-butoxy- 118 C6H14O2 000111-76-2 78 Abundance Scan 355 (7.427 min): 00702.D (-) m/z 57.10 100.00% 57

5000 45 87 — did- ' ' l f ' t'i r' 1 imma-r Tr 39 . 75 7.00 7.20 7.40 7.60 7.80 100 lz-> O' rn ' ' I 1 20 30 40 ----- 50 60 70 1,83.14 80 90 100 110 120 m/ z 45.10 36.55% Abundance #17833: Ethanol, 2-butoxy- (CAS) $$ 2-Butoxyethanol $$ 2-n... 57

5000 45 7.00 7.20 7.40 7.60 7.80 87 m/z 41.10 32.14%

m/z-> 01 1 1 1 1 ' ' 1 1 1 1 1 r'1! ■ ■ । ■ ■'! 20 30 40 50 60 +63—7 70 80 90 100 100

110 120 Abundance #17824: Ethanol, 2-butoxy- (CAS) $$ 2-Butoxyethanol $$ 2-n... 57 1 1 11 1ruvir । ■ > i • ■ 7.00 7.20 7.40 7.60 7.80 5000 45 m/z 87.10 19.72% 27 — 87

/z-> 33 0 ' i 1 ■ ' ■ 1 ' ' 1 1 i ' ' —

Abundance 20 30 40 50 60 ............. 1.... 100...... 120 70 80 90 100 110 #17827: Ethanol, 2-butoxy- $$ .beta.-Butoxyethanol $$ Buty... 57 118

7.00 m/z . i 7.20 75.00 7.40 7.60 7.80 9.20% 5000 45

27 87 75

m/z-> 0- 20 30 .. P 40 50 - 60 70 80 90 100

100 110 ng

120 7.00 7.20 7.40 7.60' '7.80

0702.D SCAN508.M Thu Jan 17 08:17:22 2002 Page 6

NYC-WTC_000051904

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NYC-WTC_000051904Source: NYC Law Department, mirrored locally

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