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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02

Page image
Scanned page image, NYC-WTC_000003303
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02JAN22\01037.D Vial: 15 Acq On : 22 Jan 2002 8:58 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclotrisiloxane, hexamethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 21.11 0.07 ug/L 19272 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 72 2 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 9 3 1-Benzopyrylium, 2-phenyl- 207 C15H11O 014051-53-7 7 4 2-Methyl-7-henvlindole 207 C15H13N 000000-00-0 7 ~dance Scan 1558 (21.105 min): 01037.D(-) m Z 207. 05 100 . 00o 27

5000

96 191 20.80 21.00 21.20 21.40 44 119133 177 m z 208.05 29.09 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 dance #70586: Cyclotrisiloxane, hexamethyl- 27

5000 20.80 21.00 21.20 21.40 m z . 96 133147 163177191 75 119 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 dance #48300: Arsenous acid, tris(trimethylsilyl) ester 27

0.80 21.00 21.20 21.40 5000 m/z 16

73 105 133 44 147 191 327 Ii 223 239 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 iance~ #24651: 1-Benzopyryliu, 2-phenyl-

m/Z LUU.is U.5tio

5000 36 131 178 102 152 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 20.80 21.00 21.20 21.40

01037.D HP010802.M Wed Jan 23 09:48:22 2002 Page 3 NYC-WTC 000003303

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NYC-WTC_000003303Source: NYC Law Department, mirrored locally

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