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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02

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Scanned page image, NYC-WTC_000003280
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\00916.D Vial: 11 Acq On : 22 Jan 2002 5:46 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 5 Silane, trichloro(.alpha.-chlo Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 36.85 0.04 ug/L 13726 1,4-DICHLOROBENZENE-D4 31.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Silane, trichloro(.alpha.-chloro-p- 258 C7H6Cl4Si 013688-90-9 9 2 4,4'-Trimethylenebis(1-methylpiperi 238 C15H30N2 064168-11-2 9 3 1,2,3-Trichloro-4-nitrobenzene 225 C6H2C13NO2 017700-09-3 5 A n A r' ..-.__1 , -1 r_ 4--..-1 .-. -.4..-. n 11 c f"n 1t 11 -]TT'.) ( A 1 •7n n _ n - )

undance Scan 2909 (36. 9 n): 0916.D (-) m Z . o 25 kU

40

5000 96 118 262

83 143 190 207 36.60 36.80 37.00 37.20 m z z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 undance #35388: Silane, trichloro(.alpha:chloro-p-tolyl)- 2

125 5000 89 63 36.60 36.80 37.00 37.20 m z 226.85 66.b6 260 189

/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 undance #31602: 4,4'-Trimethylenebis(1-methylpiperidine) 23 96 70 36.60 36.80 37.00 37.20 44 m z o 5000 140 238 58 112 126 168 194 208 z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 undance #28791: 1,2,3-Trichloro-4-nitrobenzene 169 195 2 36.60 36.80 37.00 37.20 143 m Z 261.75 44.TI% 1 109 30 5000

i ' i i i z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 36.60 36.80 37.00 37.20

00916.D HP010802.M Wed Jan 23 09:39:57 2002 Page 5

NYC-WTC 000003280

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NYC-WTC_000003280Source: NYC Law Department, mirrored locally

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