Volatile organic compounds blank results, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR01\03924D.D Vial: 26 Acq On : 2 Mar 2002 6:59 am Operator: Sample : nyc dup Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanone, 1,1,3-trichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 18.47 0.04 ug/L 12462 1,4-DIFLUOROBENZENE 15.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,3-trichloro- 160 C3H3C130 000921-03-9 4 2 Acetamide, 2-fluoro- 77 C2H4FNO 000640-19-7 3 3 Propane, l-chloro-2-nitro- 123 C3H6C1NO2 002425-66-3 2 4 Propane, 2-chloro-2-nitro- 123 C3H6C1NO2 000594-71-8 2 Abundance Scan 1340 (18.473 min): 03924D.D (-) m/z 77.00 100.00% 77 41 55 5000

91 A 1 • i ■ 1 WAAA , 18.20 18.40 18.60 18.80 m/Z 41.05 66.67% ■ । •1 ■ ■ । * 4 ’.B i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ‘ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i1 ‘ ■ i ■ ■ • ■ i miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #12245:2-Propanone, 1,1,3-trichloro- 77

5000 . 18.20 18.40 18.60 18.80 m/Z 44.05 54.62% 49

■n/z-> 20 -35.14 TIt61 — 30 42

40 50 60 i 5 99 In 70 60 90 100 110 120 130 140 150 160 162 wokonywa/ Abundance #387: Acetamide, 2-fluoro- 44

77 . 18.20 18.40 18.60 18.80 m/Z 55.U5 50.08% 5000

33 60 / * totm 11 ■' ■ • i ■ ■ ■' i'1 ■ • i ■ ■ ■ ■ i ■ ■ ■' i''' ■ i ‘ ‘ " i ‘ ’ i * ■ * ■ I

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #3997: Propane, 1-chloro-2-nitro- 77 . 18.20 18.40 18.60 18.80 m/Z 78.95 4 7.42%

5000 49

61 - TIT 90 100 110 120 130 140 150 160 ■ ■ i ■ • • • i ■ ■ i ■ ■ ■ ■ i ■ ■ m/z—> 20 30 40 50 60 70 80 18.20 18.40 18.60 18.80

03924D.D HP021102.M Mon Mar 04 13:51:13 2002 Page 3

NYC-WTC_000020640