VOC analysis results, sample AE03934, Feb 27 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB27\03934D.D Vial: 10 Acq On : 27 Feb 2002 4:18 pm Operator: Sample : nyc dup Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propane, 1,2-dichloro-2-methyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 16.34 0.04 ug/L 17534 1,4-DIFLUOROBENZENE 15.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 1,2-dichloro-2-methyl- 126 C4H8C12 000594-37-6 9 2 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 4 3 Propane, 1-chloro- 78 C3H7C1 000540-54-5 4 4 Ethyl diazoacetate 114 C4H6N2O2 000623-73-4 3 Abundance Scan 1155 (16.343 mln): 03934D.D (-) m/z 114.05 100.00% 1 4

5000 63 88 16-00 16.20 16.40 16.60 ......... 48,59,57,166 ..... 190,1?.. 100 __________ L m/Z 88.05 22.34% m/z-> Abundance 20 30 40 50 60 70 80 #4389: Propane, 1,2-dlchloro-2-methyl- 1’’I+ 110 120 I v 41

5000 27 63 MAL 16.00 16.20 16.40 16.60 m/Z 63.05 21.40% 49 77

miz-> 20 1 35——Egndum 11d—dnn— 30 .1 40 50 60 70 ill 80 90 93 111 G 1‘* ' 1 i ‘ 100 110 120 % W Abundance #2940: 1-(Propenylthio)prop-1-ene 1 4 41 99 16-00 16.20 16.40 16.60

l MM m/Z 78.05 11.36% 5000

. 59 73 85

m/z-> 20 ■ i ■ ■ ■ ■ i ■ ■ ■ • i‘ ■ 30 40 47.1157 50 60 ...70II. 1 ' I 1 1 1 1 I 1 1 1 1 I 1 1 ' 1 1 1 80 90 100 110 1 120 Abundance #62624: Propane, 1-chloro- 42 16-00 16.20 16.40 16.60 m/z 67.95 8.81%

5000 29

37 49 63 78 TP- 1. ■ i ' ' ■ । I ■ ■ ■ ■ i ■ ■ • ' i ■ ' ‘ ' i ■ ' ■ ' i 1 ‘ rrrrfr ' ’I’ ' ■ ■ i 1 ■ ■ i ■ ■ 11 m/z—> 20 30 40 50 60 70 80 90 100 110 120 16.00 16.20 16.40 16.60

03934D.D HP021102.M Thu Feb 28 10:39:45 2002 Page 4 NYC-WTC_000020489