WTC sample cover sheet, Dec 31 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\01DEC31\123lC10B.D Vial: 9 Acq On : 31 Dec 2001 6:25 pm Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 3 14:14 2002 Quant Results File: HP121001.RES

Quant Method : C:\HPCHEM\1\METHODS\HP12100l.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 03 14:14:40 2002 Response via : Initial Calibration DataAcq Meth : HP121001

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.15 75 493574 9.74 ug/L 99 35) TOLUENE 17.91 91 1408884 9.90 ug/L 100 36) TRANS-1,3-DICHLOROPROPENE 18.19 75 407354 10.35 ug/L 98 37) 1,1,2-TRICHLOROETHANE 18.56 97 196544 10.09 ug/L 98 38) TETRACHLOROETHENE 19.33 166 326727 9.74 ug/L 99 39) 1,3-DICHLOROPROPANE 19.09 76 373728 9.93 ug/L 98 40) DIBROMOCHLOROMETHANE 19.75 129 246797 10.42 ug/L 98 41) 1,2-DIBROMOETHANE 20.21 107 175580 9.47 ug/L 98 42) CHLOROBENZENE 21.10 112 922989 9.75 ug/L 99 43) 1,1,1,2-TETRACHLOROETHANE 21.13 131 322228 10.45 ug/L 97 44) 2-HEXANONE 18.48 43 103165 9.21 ug/L 98 45) ETHYLBENZENE 21.13 91 1838342 10.49 ug/L 99 46) P & M-XYLENE 21.30 106 1373929 20.87 ug/L 99 47) O-XYLENE 22.26 91 1571089 11.25 ug/L 99 48) STYRENE 22.33 104 1175133 10.82 ug/L 98 49) 1,1,2,2-TETRACHLOROETHANE 23.33 83 265288 12.73 ug/L 99 51) BROMOFORM 23.16 173 139193 8.20 ug/L 97 52) ISOPROPYLBENZENE 22.99 105 1921469 7.83 ug/L 97 53) 1,2,3-TRICHLOROPROPANE 23.66 110 70665 7.90 ug/L 98 54) N-PROPYLBENZENE 23.86 91 2658245 8.36 ug/L 98 55) BROMOBENZENE 24.08 156 438970 8.40 ug/L 90 56) 1,3,5-TRIMETHYLBENZENE 24.17 105 1721115 8.12 ug/L 99 57) 2-CHLOROTOLUENE 24.32 91 1544096 7.65 ug/L 95 58) 4-CHLOROTOLUENE 24.40 91 1702019 9.42 ug/L 98 59) TERT-BUTYLBENZENE 24.97 134 391020 8.64 ug/L 90 60) 1,2,4-TRIMETHYLBENZENE 25.05 105 1860200 8.46 ug/L 99 61) SEC-BUTYLBENZENE 25.41 105 2566896 8.70 ug/L 98 62) P-ISOPROPYLTOLUENE 25.68 119 2071887 8.75 ug/L 98 63) 1,3-DICHLOROBENZENE 26.02 146 1067991 9.46 ug/L 98 64) 1,4-DICHLOROBENZENE 26.23 146 1043784 9.24 ug/L 98 65) N-BUTYLBENZENE 26.55 91 2236845 9.87 ug/L 99 66) 1,2-DICHLOROBENZENE 27.08 146 907855 9.74 ug/L 97 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.72 157 44928 9.43 ug/L 90 68) NITROBENZENE 28.92 77 362914 184.77 ug/L 95 69) 1,2,4-TRICHLOROBENZENE 30.66 180 514577 9.96 ug/L 100 70) HEXACHLOROBUTADIENE 30.91 225 293951 9.36 ug/L 98 71) NAPHTHALENE 31.32 128 564572 9.91 ug/L 100 72) 1,2,3-TRICHLOROBENZENE 31.88 180 371481 9.80 ug/L 98

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1231C10B.D HP121001.M Thu Jan 03 14:15:05 2002 Page 2

NYC-WTC 000002883