WTC sample cover sheet, Dec 14 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\Oldecl7\1217C10.D Vial: 8 Acq On : 17 Dec 2001 9:36 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Dec 17 10:15 2001 Quant Results File: HP121001.RES

Quant Method : C:\HPCHEM\1\METHODS\HP121001.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Dec 12 08:39:59 2001 Response via : Initial Calibration DataAcq Meth : HP121001

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.11 75 711711 9.48 ug/L 99 35) TOLUENE 17.88 91 2013571 9.56 ug/L 99 36) TRANS-1,3-DICHLOROPROPENE 18.15 75 569306 9.77 ug/L 97 37) 1,1,2-TRICHLOROETHANE 18.53 97 272742 9.45 ug/L 98 38) TETRACHLOROETHENE 19.31 166 451398 9.09 ug/L 97 39) 1,3-DICHLOROPROPANE 19.06 76 541822 9.72 ug/L 99 40) DIBROMOCHLOROMETHANE 19.74 129 339965 9.69 ug/L 96 41) 1,2-DIBROMOETHANE 20.18 107 254352 9.26 ug/L 97 42) CHLOROBENZENE 21.07 112 1318083 9.41 ug/L 99 43) 1,1,1,2-TETRACHLOROETHANE 21.10 131 439754 9.62 ug/L 98 44) 2-HEXANONE 18.44 43 181549 10.94 ug/L 99 45) ETHYLBENZENE 21.12 91 2572918 9.91 ug/L 98 46) P & M-XYLENE 21.27 106 1851275 18.99 ug/L 97 47) O-XYLENE 22.24 91 2098748 10.15 ug/L 99 48) STYRENE 22.29 104 1568211 9.75 ug/L 99 49) 1,1,2,2-TETRACHLOROETHANE 23.32 83 312312 10.12 ug/L 98 51) BROMOFORM 23.13 173 173796 9.00 ug/L 98 52) ISOPROPYLBENZENE 22.96 105 2478144 8.88 ug/L 99 53) 1,2,3-TRICHLOROPROPANE 23.64 110 89772 8.83 ug/L 94 54) N-PROPYLBENZENE 23.83 91 3302888 9.13 ug/L 100 55) BROMOBENZENE 24.05 156 518880 8.73 ug/L 98 56) 1,3,5-TRIMETHYLBENZENE 24.15 105 2188322 9.08 ug/L 99 57) 2-CHLOROTOLUENE 24.30 91 2151435 9.38 ug/L 97 58) 4-CHLOROTOLUENE 24.37 91 1930763 9.40 ug/L 100 59) TERT-BUTYLBENZENE 24.93 134 466183 9.06 ug/L 99 60) 1,2,4-TRIMETHYLBENZENE 25.02 105 2286974 9.15 ug/L 99 61) SEC-BUTYLBENZENE 25.39 105 3094320 9.22 ug/L 98 62) P-ISOPROPYLTOLUENE 25.65 119 2471240 9.17 ug/L 100 63) 1,3-DICHLOROBENZENE 25.99 146 1168968 9.10 ug/L 100 64) 1,4-DICHLOROBENZENE 26.21 146 1169407 9.10 ug/L 99 65) N-BUTYLBENZENE 26.54 91 2584660 10.03 ug/L 99 66) 1,2-DICHLOROBENZENE 27.05 146 995646 9.39 ug/L 99 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.70 157 51649 9.53 ug/L 97 68) NITROBENZENE 28.89 77 444881 199.19 ug/L 97 69) 1,2,4-TRICHLOROBENZENE 30.62 180 556675 9.47 ug/L 99 70) HEXACHLOROBUTADIENE 30.88 225 332295 9.31 ug/L 98 71) NAPHTHALENE 31.31 128 604812 9.34 ug/L 98 72) 1,2,3-TRICHLOROBENZENE 31.85 180 403379 9.35 ug/L 98

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1217C10.D HP121001.M Mon Dec 17 10:15:32 2001 Page 2

NYC-WTC 000002156