WTC sample cover sheet, Dec 19 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\01dec21\1221C10.D Vial: 8 Acq On : 21 Dec 2001 9:56 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Dec 21 10:34 2001 Quant Results File: HP121001.RES

Quant Method : C:\HPCHEM\1\METHODS\HP121001.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Dec 20 09:38:26 2001 Response via : Initial Calibration DataAcq Meth : HP121001

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.15 75 414478 9.35 ug/L 99 35) TOLUENE 17.91 91 1127405 9.05 ug/L 100 36) TRANS-1,3-DICHLOROPROPENE 18.19 75 343824 9.99 ug/L 99 37) 1,1,2-TRICHLOROETHANE 18.56 97 166594 9.77 ug/L 96 38) TETRACHLOROETHENE 19.34 166 258525 8.81 ug/L 98 39) 1,3-DICHLOROPROPANE 19.09 76 323437 9.82 ug/L 98 40) DIBROMOCHLOROMETHANE 19.77 129 207728 10.02 ug/L 96 41) 1,2-DIBROMOETHANE 20.21 107 147023 9.06 ug/L 100 42) CHLOROBENZENE 21.10 112 747935 9.03 ug/L 99 43) 1,1,1,2-TETRACHLOROETHANE 21.13 131 267868 9.92 ug/L 97 44) 2-HEXANONE 18.48 43 98772 10.07 ug/L 99 45) ETHYLBENZENE 21.15 91 1464620 9.55 ug/L 98 46) P & M-XYLENE 21.30 106 1051306 18.25 ug/L 97 47) O-XYLENE 22.28 91 1228722 10.05 ug/L 98 48) STYRENE 22.33 104 916342 9.64 ug/L 99 49) 1,1,2,2-TETRACHLOROETHANE 23.35 83 205109 11.24 ug/L 96 51) BROMOFORM 23.16 173 119100 8.35 ug/L 98 52) ISOPROPYLBENZENE 22.99 105 1458829 7.08 ug/L 99 53) 1,2,3-TRICHLOROPROPANE 23.67 110 56930 7.58 ug/L 96 54) N-PROPYLBENZENE 23.86 91 2011261 7.53 ug/L 99 55) BROMOBENZENE 24.08 156 333744 7.60 ug/L 99 56) 1,3,5-TRIMETHYLBENZENE 24.18 105 1317624 7.40 ug/L 98 57) 2-CHLOROTOLUENE 24.34 91 1319475 7.79 ug/L 96 58) 4-CHLOROTOLUENE 24.40 91 1234181 8.13 ug/L 99 59) TERT-BUTYLBENZENE 24.97 134 294200 7.74 ug/L 96 60) 1,2,4-TRIMETHYLBENZENE 25.05 105 1427809 7.73 ug/L 99 61) SEC-BUTYLBENZENE 25.43 105 1952272 7.88 ug/L 97 62) P-ISOPROPYLTOLUENE 25.68 119 1615234 8.11 ug/L 98 63) 1,3-DICHLOROBENZENE 26.02 146 801149 8.44 ug/L 99 64) 1,4-DICHLOROBENZENE 26.24 146 808339 8.52 ug/L 98 65) N-BUTYLBENZENE 26.57 91 1714032 9.00 ug/L 98 66) 1,2-DICHLOROBENZENE 27.08 146 697900 8.91 ug/L 99 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.73 157 37143 9.28 ug/L 90 68) NITROBENZENE 28.92 77 312690 189.48 ug/L 95 69) 1,2,4-TRICHLOROBENZENE 30.66 180 410023 9.44 ug/L 99 70) HEXACHLOROBUTADIENE 30.91 225 240812 9.13 ug/L 99 71) NAPHTHALENE 31.34 128 459995 9.61 ug/L 98 72) 1,2,3-TRICHLOROBENZENE 31.88 180 301904 9.47 ug/L 96

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1221C10.D HP121001.M Fri Dec 21 10:35:09 2001 Page 2

NYC-WTC 000002395