Volatile organic compound analysis results, sample AD27764, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\Olnovl6\1116R40.D Acq On Vial: 7 : 16 Nov 2001 11:07 am Operator: 206-BH Sample : ref 40 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 16 11:46 2001 Quant Results File: HP110101.RES Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-DICLUOROBENZENE ------------------------------------ 14.44 114 772528 5.00 ug/L 0.00 22) CHLOROBENZENE-D5 21.02 117 739342 5.00 ug/L -0.02 50) 1,4-DICHLOROBENZENE-D4 26.18 152 368497 5.00 ug/L -0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.64 65 235579 5.17 ug/L -0.02 Spiked Amount 5.000 Recovery = 103.400 3) 4-BROMOFLUOROBENZENE 23.59 174 246846 6.15 ug/L -0.02 Spiked Amount 5.000 Recovery = 123.000 23) TOLUENE-D8 17.74 98 993317 4.45 ug/L 0.00 Spiked Amount 5.000 Recovery = 89.00% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.47 85 989182 47.93 ug/L 100 5) CHLOROMETHANE 4.97 50 729170 36.66 ug/L 98 6) VINYL CHLORIDE 5.11 62 522863 34.75 ug/L 98 7) BROMOMETHANE 6.06 94 685645 36.40 ug/L 99 8) CHLOROETHANE 6.20 64 504248 37.26 ug/L 98 9) TRICHLOROFLUOROMETHANE 6.74 101 1646994 49.75 ug/L 99 10) ACETONE 7.66 43 173796 41.52 ug/L 94 11) 1,1-DICHLOROETHENE 8.00 61 2038212 51.22 ug/L 94 12) METHYLENE CHLORIDE 8.99 49 1885897 43.42 ug/L 99 13) METHYL TERT BUTYL ETHER 9.28 73 2192414 29.75 ug/L 99 14) TRANS-1,2-DICHLOROETHENE 9.64 61 2151192 48.20 ug/L 99 15) 1,1-DICHLOROETHANE 10.50 63 2661108 45.55 ug/L 99 16) 2-BUTANONE (MEK) 11.32 43 330238 38.94 ug/L 95 17) 2,2-DICHLOROPROPANE 11.71 77 2265788 51.60 ug/L 99 18) CIS-1,2-DICHLOROETHENE 11.80 96 1441540 45.83 ug/L 94 19) CHLOROFORM 12.14 83 2493396 47.79 ug/L 98 20) BROMOCHLOROMETHANE 12.50 49 1199612 45.95 ug/L 99 21) 1,2-DICHLOROETHANE 13.84 62 1548878 48.62 ug/L 99 24) 1,1,1-TRICHLOROETHANE 13.03 97 2074615 47.16 ug/L 99 25) 1,1-DICHLOROPROPENE 13.37 75 2145086 44.62 ug/L 99 26) CARBON TETRACHLORIDE 13.60 117 1772420 52.40 ug/L 100 27) BENZENE 13.96 78 6216952 41.32 ug/L 100 28) TRICHLOROETHENE 15.22 95 1565259 44.32 ug/L 93 29) 1,2-DICHLOROPROPANE 15.56 63 1624576 40.85 ug/L 100 30) DIBROMOMETHANE 16.21 174 472821 49.25 ug/L 96 31) BROMODICHLOROMETHANE 16.06 83 1798447 45.19 ug/L 99 32) 2-CHLOROETHYL VINYL ETHER 16.57 63 535752 47.53 ug/L 97 33) Methyl iso-butyl ketone 16.64 58 266659 44.00 ug/L 87 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1116R40.D HP110101.M Fri Nov 16 11:46:27 2001 Page 1

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