Volatile organic compound analysis results, sample AD27490, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\Olnovl4\1114C10A.D Vial: 11 Acq On : 14 Nov 2001 4:34 pm Operator: Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 14 17:13 2001 Quant Results File: HP110101.RES

Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-DIFLUOROBENZENE 14.40 114 649156 5.00 ug/L -0.04 22) CHLOROBENZENE-D5 21.00 117 575557 5.00 ug/L -0.04 50) 1,4-DICHLOROBENZENE-D4 26.16 152 265181 5.00 ug/L -0.04 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.62 65 207913 5.43 ug/L -0.04 Spiked Amount 5.000 Recovery = 108.600 3) 4-BROMOFLUOROBENZENE 23.57 174 174858 5.18 ug/L -0.04 Spiked Amount 5.000 Recovery = 103.60% 23) TOLUENE-D8 17.73 98 852619 4.91 ug/L -0.02 Spiked Amount 5.000 Recovery = 98.20%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.46 85 255707 14.74 ug/L 98 5) CHLOROMETHANE 4.96 50 251400 15.04 ug/L 99 6) VINYL CHLORIDE 5.13 62 163062 12.90 ug/L 100 7) BROMOMETHANE 6.05 94 151779 9.59 ug/L 98 8) CHLOROETHANE 6.18 64 136311 11.99 ug/L 96 9) TRICHLOROFLUOROMETHANE 6.73 101 352001 12.65 ug/L 99 10) ACETONE 7.64 43 46966 13.35 ug/L 96 11) 1,1-DICHLOROETHENE 8.00 61 479406 14.34 ug/L 95 12) METHYLENE CHLORIDE 8.97 49 506691 13.88 ug/L 94 13) METHYL TERT BUTYL ETHER 9.28 73 466607 7.53 ug/L 95 14) TRANS-1,2-DICHLOROETHENE 9.62 61 506181 13.50 ug/L 95 15) 1,1-DICHLOROETHANE 10.50 63 630272 12.84 ug/L 99 16) 2-BUTANONE (MEK) 11.32 43 68061 9.55 ug/L 95 17) 2,2-DICHLOROPROPANE 11.70 77 472607 12.81 ug/L 97 18) CIS-1,2-DICHLOROETHENE 11.78 96 322131 12.19 ug/L 88 19) CHLOROFORM 12.12 83 561045 12.80 ug/L 99 20) BROMOCHLOROMETHANE 12.48 49 300442 13.70 ug/L 86 21) 1,2-DICHLOROETHANE 13.82 62 346268 12.93 ug/L 98 24) 1,1,1-TRICHLOROETHANE 13.01 97 429448 12.54 ug/L 100 25) l,1-DICHLOROPROPENE 13.35 75 442096 11.81 ug/L 99 26) CARBON TETRACHLORIDE 13.59 117 337827 12.83 ug/L 99 27) BENZENE 13.94 78 1344256 11.48 ug/L 100 28) TRICHLOROETHENE 15.20 95 303583 11.04 ug/L 100 29) 1,2-DICHLOROPROPANE 15.55 63 363750 11.75 ug/L 99 30) DIBROMOMETHANE 16.19 174 87559 11.72 ug/L 88 31) BROMODICHLOROMETHANE 16.04 83 372487 12.02 ug/L 99 32) 2-CHLOROETHYL VINYL ETHER 16.55 63 105763 12.05 ug/L 99 33) Methyl iso-butyl ketone 16.62 58 56466 11.97 ug/L 83 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1114C10A.D HP110101.M Wed Nov 14 17:13:21 2001 Page 1

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