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← Document results/DEP Box 04/524 11/13/01
Document / 91 pages

Volatile organic compound analysis results, sample AD27113, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report listing recovery percentages for volatile organic compounds in sample AD27113 from November 13, 2001.

NYC-WTC_000001026–000001116

Folder label: “524 11/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\Olnov9\1109R40.D Vial: 7 Acq On : 10 Nov 2001 9:32 am Operator: Sample : ref 40 Inst : GC/MS Ins Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 10 10:11 2001 Quant Results File: HP1l0101.RES Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response •Conc Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 14.41 114 456152 5.00 ug/L -0.03 22) CHLOROBENZENE-D5 21.00 117 434397 5.00. ug/L -0.03 50) 1,4-DICHLOROBENZENE-D4 26.16 152 223746 5.00 ug/L -0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.62 65 163986 6.09 ug/L -0.03 Spiked Amount 5.000 Recovery = 121.800 3) 4-BROMOFLUOROBENZENE 23.57 174 150006 6.33 ug/L -0.03 Spiked Amount 5.000 Recovery = 126.60% 23) TOLUENE-D8 17.73 98 621829 4.74 ug/L -0.02 Spiked Amount 5.000 Recovery = 94.80% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.46 85 355471 29.17 ug/L 99 5) CHLOROMETHANE 4.97 50 604662 51.49 ug/L 99 6) VINYL CHLORIDE 5.10 62 266960 30.05 ug/L 98 7) BROMOMETHANE 6.05 94 430255 38.68 ug/L 98 8) CHLOROETHANE 6.18 64 347690 43.51 ug/L 97 9) TRICHLOROFLUOROMETHANE 6.73 101 822850 42.09 ug/L 99 10) ACETONE 7.66 43 137015 55.44 ug/L 94 11) 1,1-DICHLOROETHENE 7.98 61 1086898 46.26 ug/L 91 12) METHYLENE CHLORIDE 8.97 49 1236079 48.20 ug/L 92 13) METHYL TERT BUTYL ETHER 9.26 73 1357027 31.19 ug/L 98 14) TRANS-1,2-DICHLOROETHENE 9.62 61 1315985 49.94 ug/L 94 15-)- 1,-1-DICHLOROETHANE 10.50 --- 63 16-56-645- --

4802ugtL 99- 16) 2-BUTANONE (MEK) 11.32 43 226227 45.18 ug/L 95 17) 2,2-DICHLOROPROPANE 11.70 77 820232 31.64 ug/L 97 18) CIS-1,2-DICHLOROETHENE 11.78 96 834947 44.95 ug/L 84 19) CHLOROFORM 12.12 83 1487711 48.29 ug/L 99 20) BROMOCHLOROMETHANE 12.50 49 781386 50.69 ug/L 95 21) 1,2-DICHLOROETHANE -- 13.83 6-2 984425 -----52.33 ug/L -99- -- 24) 1,1,1-TRICHLOROETHANE 12.99 97 1163216 45.00 ug/L 99 25)-_1,1-DICHLOROPROPENE 13.33 75 1154653 40.88 ug/L 98-- - 13.5-7 . .17 - 899331-. --45.26 _ug/L -.--_2161_ CARBON TETRACHLOR-IDE- - - 27 BENZENE 3515709= 13.93-" 7B - 39.77 -ug/L

28) TRICHLOROETHENE 15.19 95 857112. 41.31 ug/L 98 29) 1,2-DICHLOROPROPANE 15.55 63 995867 42.62 ug/L 99 - _.`- . h&: 1 `74_ 244106 43 .28 ug/Z

31) BROMODICHLOROMETHANE 16.04 83 1053766 .45.06 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.55 63 332487 50.20 ug/L 99 33) Methyl iso-butyl ketone 16.62 58 173441 48.70 ug/L 81 -------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1109R40.D HP110101.M Sat Nov 10 10:11:08 2001 Pagel

NYC-WTC 000001039

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