NYC-WTC_000234032

NYC 9/11 Public Portal Document

<date> PASC - Certificate of Analysis Page 3 of

R02090951 R02090951 R02090951 R02090951 Client ID: 06A 07A OSA 09A Lab No.: 060272 02 060273 02 060274 02 060275 02 Sampled: 12-Scp-2002 12-Scp-2002 12-Scp-2002 12-Scp-2002 Component MDL Units

Total Tctrachlorodibcnzofurans pg 5.8 <1.7 <1.7 4.8 Total Pentachlorodibenzofurans <1.5 <1.6 <1.7 <9.5 Total Hexachlorodibenzofurans 2..5 <1.1 1.8 <4.1 Total Heptachlorodibenzofurans 11 <2.1 <3.8 <6.3 Octachlorodibenzofuran 9.6 4.2 Total Tetrachlorodibenzo-p-dioxins 20 <1.3 <2.0 10 Total Pentachlorodibenzo-p-dioxins <3.4 <2.9 <2.6 <5.9 Total Hexachlorodibenzo-p-dioxins 1.7 <3.7 1.9 <16 Total Heptachlorodibenzo-p-dioxins 9.8 <2.0 4.2 7.7 Octaclilorodibenzo-p-dioxin 68 8.6 12 46 Internal Recoveries % 2,3,7,8-T4CDF-13C12 72 75 71 81 2,3,7,8-T4CDD-13C12 85 92 83 76 1,2,3,7.8-P5CDF-13C12 67 83 70 74 1,2,3,7.8-P5CDD-13C12 76 91 79 79 1,2,3,4.7,8-H6CDF-13C12 86 96 90 79 1,2,3,6.7,8-H6CDD-13C12 90 95 94 82 1,2,3,4.6,7,8-H7CDF-13C12 92 97 92 77 1,2,3,4.6,7,8-H7CDD-13C12 93 97 97 78 OCDD-13C12 104 112 114 68

2,3,7,8-C14-Dibenzofiiran (DB5) pg 4.0 <1.7 <1.7 <4.8 2,3,7,8-C14-Dibenzo-p-dioxin <1.3 <1.3 <2.0 <5.9 1,2,3,7,8-C15-Dibenzofuran <1.5 <1.6 <9.2 2,3,4,7,8-C15-Dibenzofuran <1.6 <1.6 <1.8 <9.8 l,2,3,7.8-C15-Dibenzo-p-dioxin <2.8 <2.9 <2.6 <5.9 1,2,3,4,7,8-C16-Dibcnzofuran <0.92 <0.97 1.6 <4.1 1,2,3,6,7,8-C16-Dibenzofuran <0.94 <0.99 <0.86 <3.4 2,3,4,6,7,8-C16-Dibenzofuran <1.1 <1.2 <1.0 <4.4 1,2,3,7,8,9-C16-Dibcnzofuran <1.4 <1.4 <1.2 <4.8 1,2,3,4,7,8-C16-Dibenzo-p-dioxin <1.2 <1.6 <1.4 <20 1,2,3,6,7,8-C16-Diben/o-p-dioxin <1.2 <1.6 <1.4 <14 1,2,3,7,8,9-C16-Dibenzo-p-dioxin <1.2 <1.6 <1.3 <15 1,2,3,4,6,7,8-C17-Dibenzofuran 5.0 <3.2 <3.3 <5.5 1,2,3,4,7,8,9-C17-Dibenzofuran <2.2 <4.5 <4.6 <7.4 1,2,3,4,6,7,8-C17-Dibenzo-p-dioxin 9.8 <2.7 4.2 7.7 1,2,3,4.6,7,8,9-C18-Dibenzofuran 9.6 4.2 l,2,3,4,6,7,8,9-C18-Dibenzo-p-dioxin 68 8.6 12 46

2,3,7,8-TCDF (DB225) pg <5.7 <3.1 <3.7 <4.8 Internal Recoveries % 2,3,7,8-TCDF-13C12 96 92 92 81

TEQ based on Nato Factors pg 2.7 2.4 2.8 11.2

Client:Philip Analytical Services Inc Project:Misc.

CITY_21MC100_003231107

NYC-WTC_000234035