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PCDD/PCDF wipe sample results, PS 234M, Feb 2002
Machine-extracted title · confidence 95%Laboratory report presenting analysis results for polychlorinated dibenzo-p-dioxins and dibenzofurans from a wipe sample collected at PS 234M.
NYC-WTC_000177808–000177810Page image
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NYC 9/11 Public Portal Document
FEB-19-D2 14:27 FROM-PACE ANALYTICAL 612-607-6444 T-556 P.06/06 F-681 1700 Elm Street - Suite 200 TW Minneapolis, MN 55414
^ceAnalvtical Method 8290 Analysis Results Tai: S12-607-1700
Client-ATC Client's Sample ID ATC-Q129-234M-DX3 Lab Sample ID 103297024 Filename U20214A_11 injected By CVS Total Amount Extracted 1 m2 Matrix WIPE % Moisture NA Dilution NA Dry Weight Extracted NA Collected 01/29/2002 ICAL Date 01/25/2002 Received 01/31/2002 CCal Filename(s) U20214X.02 & U20214A_16 Extracted 02/11/2002 Method Blank ID BLANK-1458 Analyzed 02/14/2002 20:12 Native Cone EMPC LRL Internal ng's Percent Isomers ng/in2 ng/m2 ng/m2 Standards Added Recovery 2.3,7,8-TCDF ND 0.0041 A 2,3,7,8-TCDF-13C 2.00 63 Total TCDF nd 0.0020 2.3.7.8-TCDD-13C 2.00 73 1,2,3,7,8-PeCDF-13C 2.00 65 2,3,7,8-TCDD ND 0.0072 A' 2,3,4.7,8-PeCDF-13C 2.00 64 Total TCDD ND 0.0020 1,2,3,7,8-PeCDD-13C 2.00 86 1.2,3,4,7,8-HxCDF-13C 2.00 86 1,2,3,7.8-PeCDF ND 0.0100 1.2,3,6,7,8-HxCDF-13C 2.00 75 2.3.4,7,8-PeCDF ND 0.0100 2,3,4,6,7,8-HxCDF-13C 2.00 75 Total PeCDF ND 0.0100 1,2,3,7,8,9-HxCDF-13C 2.00 80 1,2.3.4.7.8-HxCDD-13C 2.00 93 1.2,3,7,8-PeCDD ND 0.0100 1.2,3,6,7,8-HxCDD-13C 2.00 84 Total PeCDD ND 0.0100 1.2.3,4,6,7,8-HpCDF-13C 2.00 87 1,2,3,4,7,8,9-HpCDF-13C 2.00 84 1,2,3,4,7,8-HxCDF ND 0.0100 1,2,3,4,6,7,8-HpCDD-13C 2.00 80 1,2,3,6,7.8-HxCDF ND 0.0100 OCDD-13C 4.00 74 2,3,4,6,7,8-HxCDF ND 0.0100 1,2,3.7.8,9-HxCDF ND 0.0100 1,2,3.4-TCDD-13C 2.00 NA Total HxCDF ND 0.0100 1,2,3,7,8,9-HxCDD-13C 2.00 NA
1,2,3,4,7.8-HxCDD ND 0.0100 2,3,7,8-TCDD-37CI4 0.20 80 1,2,3,6,7,8-HxCDD ND 0.0100 1,2,3,7,8,9-HxCDD ND 0.0100 Total HxCDD ND 0.0100 1,2,3,4,6,7,8-HpCDF ND 0.0100 Total 2,3,7,B-TCDD 1,2,3.4.7.8.9-HpCDF ND 0.0100 Equivalence: 0.00 ng/m2 Total HpCDF ND 0.0100 (Using ITE Factors) 1,2,3,4,6,7,8-HpCDD ND 0.0100 Total HpCDD ND 0,0100 OCDF ND 0.0200 OCDD ND 0.0200
LRL = Lower Reporting Limit Cone = Concentration (Totals include 2,3.7,8-subatitutad isomers) I = Interference EMPC = Estimated Maximum Possible Concentration E = PCDE Interference A s Detection Limit based on signai-to-noise measurement S = Saturated signal J X Concentration detected is below the calibration range ND = Not Detected B = Leas than 10 times higher than method Wank level NA = Not Applicable P = Recovery outside of target range NC = Not Calculated Nn = Value obtained from additional analysis • = See Discussion Report No... 02-1053614
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
CONFIDENTIAL, CITY_21MC100_003444479
SUBJECT TO PROTECTIVE ORDER NO. 2, SEPT. 2008
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