NYC 9/11 Public Portal Document
Indoor floor dust samples will be collected using the EPA ERT SOP for household dust
collection. As much dust as possible will be collected; the area vacuumed will be measured and
reported. Samples will be analyzed for crystalline silica, gypsum, mica, and calcite using XRD
analysis. Asbestos and fibrous glass will be analyzed using New York State Method 198.1
(polarized light microscopy [PLM]); if <1% asbestos is found. New York State Method 198.4
(transmission electron microscopy [TEM]) analysis will be conducted. The pH of the dust will
be tested using EPA SW846 Method 9045C.
2. Outdoor
Outdoor air and settled dust sampling will occur in areas adjacent to the residential building
being tested indoors. Sampling will occur concurrently with indoor sampling.
Ambient air sampling will be conducted at breathing height. Air sampling for asbestos will be
conducted and analyzed using NIOSH methods 7400 and 7402. Respirable crystalline silica will
be sampled and analyzed using NIOSH method 7500. Air sampling for inhalable and thoracic
size particles will be conducted using EPA method IP-IOA. The respirable silica sample will be
used to analyze the respirable fraction of the dust. The relative amounts (percent weight) of each
fraction present will be determined. Each fraction will be analyzed for silica, gypsum, mica, and
calcite using XRD analysis, and for fibrous glass using SEM.
Settled surface dust samples will be collected by scooping visible dust into a glass container. A
minimum of 25-30 grams of sample is required. The area of the surface sampled (e.g., 100 cm’)
will be measured and documented. Samples will be analyzed for crystalline silica, gypsum,
mica, and calcite using XRD analysis, and for asbestos and fibrous glass using New York State
method 198.1 (PLM). If PLM shows less than <1% asbestos. New York State Method 198.4
(transmission electron microscopy [TEM]) analysis will be conducted. The pH of the dust will
be tested using EPA SW846 Method 9045C.
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NYC-WTC_000164791
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