NYC 9/11 Public Portal Document
DRAFTM 2. Post cleaning air samples for fibrous glass and silica shall be collected concurrently with the
asbestos clearance air sampling procedures specified herein. Five samples for fibrous glass and one
sample for silica shall be collected in each apartment.
3. Wipe samples shall be collected before and after cleaning for lead, dioxin, and PAHs.
Prior to the cleaning activities, three wipe samples shall be collected for each of these parameters in
each apartment. The sampling locations shall be a wall, a bare floor, and a counter or tabletop.
After cleaning activities, three wipe samples shall be collected for each of these parameters in each
apartment. The sampling locations shall be a wall, a bare floor, and a counter or tabletop; preferably
at the same location as the pre-cleaning samples.
4. The required sampling and analytical procedures are specified in Table 1.
5. The detection limit for PAHs shall be no greater than 1 pg/m^.
6. Samples containing concentrations of specific congeneric analytes (PCDDs and PCDFs) considered
within the scope of the dioxin sampling method that are greater than ten times the upper MCLs must
be analyzed by a protocol designed for such concentration levels, e.g.. Method 8280. Analytical
results shall be reported using a 2,3,7,8-TCDD toxicity equivalence (TEQ). The TEQs shall be
reported four ways. A TEQ which sets non-detects to zero (i.e., TEQ (ND=0), a TEQ which sets
non-detects at 1/2 the detection limit (i.e., TEQ (ND=l/2), a TEQ Estimated Maximum Potential
Concentration with non-detects set to zero (i.e., TEQ EMPC (ND=0), and a TEQ Estimated
Maximum Potential Concentration with non-detects set to 1/2 the detection limit (i.e., TEQ EMPC
(ND=l/2). Please see attachment 2 for the format and data to report for dioxin wipe samples.
Table 1: Sampling and Analytical Methods
Parameter Description Sampling Analytical Method Maximum
Methodology Turnaround
Time
Lead Wipe samples HUD Appendix 13.1 EPA Method SW-846-6010B 1 day
PAHs Wipe samples ASTM D6661-01 ASTM-6661-01 14 days
EPA SW-846-8270C
Dioxin Wipe samples ASTM 6661-01 ASTM 6661-01 14 days
EPA Method SW-846-8290
Fibrous Air samples NIOSH 7400 NIOSH 7400, 3 days
Glass Counting Method “B”
Crystalline Air samples NIOSH 7500 NIOSH 7500 (XRD) 14 days
Silica
Asbestos Air samples Collection using Asbestos Fiber Analysis by 1 day
NIOSH 7400 Transmission Electron Microscopy
(TEM) Performed by EPA 40 CRF
Part 763 Final Rule (AHERA) [see
Attachment 1] and NIOSH 7400
(PCM)
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