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← Document results/DEP Box 03/2002 E-Mail Sent M. Gilsenan
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Forwarding WTC air monitoring scope for final review, Aug 2002

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DEP official requests final review of the latest air monitoring Scope of Work to conclude negotiations.

NYC-WTC_000139257–000139330

Folder label: “2002 E-Mail Sent M. Gilsenan

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NYC 9/11 Public Portal Document

n. 763, Subpt. E, App. A 40 CFR Ch. I (7-1-00 Edition) in diameter at crossover. The microscope i. Standard repUca grating may be used to shall be calibrated routinely (see Unit III.J.) determine magnification (e.g., 2160 Unes/ for magnification and camera constant. mm). b. While not required on every microscope 11. Gold standard may be used to determine In the laboratory, the laboratory must have camera constant. either one microscope equipped with energy c. Use a specimen holder with single tilt dispersive X-ray analysis or access to an and/or double tilt capabilities. equivalent system on a TEM In another lab­ 2. Procedure. oratory. This must be an Energy Dispersive a. Start a new Count Sheet for each sample X-ray Detector mounted on TEM column and to be analyzed. Record on count sheet: ana­ associated hardware/software to collect, lyst's initials and date; lab sample number; save, and read out spectral information. client sample number microscope Identifica­ Calibration of Multi-Channel /Analyzer shall tion; magnification for analysis; number of be checked regularly for Al at 1.48 KeV and predetermined grid openings to be analyzed; Cu at 8.04 KeV, as well as the manufacturer’s and grid Identification. See the following procedures. Figure 4:

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NYC-WTC_000139307Source: NYC Law Department, mirrored locally

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