NYC 9/11 Public Portal Document
12/11/2001 17:08 FAX 212 353 8306 ATC 0 008
• D 5755
smaller components without losing its fibrous properties or 5. Significance and Use
appearance. 5.1 This microvacuum sampling and indirect analysis
3.2 Descriptions of Terms Specific to This Standard method is used for the general testing of nonairborne dust
3.2.1 aspect ratio—the ratio of the length of a fibrous samples for asbestos. It is used to assist in the evaluation of
particle to its average width. dust that may be found on surfaces in buildings such as
3.2.2 bundle—a structure composeed of three or more ceiling tiles shelving, electrical components, duct work,
fibers in a parallel arrangement with the fibers closer than carpe, etc. This test method provides an index of the
one fiber diameter to each other. concentration of asbestos structures in the dust per unit area
3.23 duster-a structure with 66ers in a random arranger analyzed as derived from a quantitative TEM analysis.
meat such that all fibers are intermixed and no single fiber is 5.1.1 This test method does not describe procedures or
isolated from the group; groupings of fibers must have more techniques required to evaluate the safety or habitability of
than two points touching. buildings with as nos.containing
materials,
or compliance
3.2,.4 debris-materials that are of an amount and size with fe deral, state,
or local regulations or
stattrsw.
It
is
the
(particles greater than I mm in diameter) that on be visually user's responsibility to make these determinations.
Identified as to their source. 5.1.2 At present, a single direct relationship between
3.2.5 durst--any material composed of particles in a size asbestos-containing dust and potential human exposure does
range of 1 mm and large enough to settle by virtue of their not exist.
Accordingly.
the
uses should consider these data in
from the ambient air (am definition for settleable
weight
re
lationship
to other available
information in
their
evalua-
particulate matter in Test Method D 1739). tion.
3.2.6 a srudum having a minimum length of 0.5 5.2 This test method uses the definition, amicable partic-
µm, an aspect ratio of 5:1 or greater, and substantially ulate material, found in Ten
Method D 1739
as
the
dcfin-
parallel sides (4). tion of dust. This definition accept$
all particles small
3.2.7 fibrous--of a mineral composed of parallel, radi- enough to pass through a 1 mm (No. 18) semen. Thus. a
ating, or interlaced aggregates of fibers, from which the fibers sing, large asides containing particle(s) (horn the large
are sometimes separable. That the exystaltine aggrepte end of the particle size distribution) d'spaaed during sample
preparation may result in anomalously large asbestos con-
is,
may be referred to as fibrous even if it is not composed of
separable'Sbers, but het that distiu cep issrsu e. The term centration results in the TEM analyses of that sample. It it,
fibrous is used in a general mineralogical way to describe
samples
ehereibre,
independent
suoonint..ded that multiple
of grains that crystallize In a needle..lke habit and
a minimum of three
are
the
secured om
fr and
area,
same
appear to be composed of fibers. Fibrous has a much more samples analysed by the entire procedure.
general r+8 than asbestos. While it is cos that all
asbestos minerals are fibrous, not all minerals having fibrous
6.
Interferences
habits am asbestos. 6.1 The following minerals have properties (that is, chem-
32.8 indirect preparations—a method in which a sample
similar
which to
are very
structure)
crystaJliue
or
ical
passes through one or more intermediate steps prior to final
may
analysis by
the
with
minerals
interfere
and
asbestos
filtration. canting a
fa lse
positive
to
be recorded during
the
test.
s for these materials must be
Therefore, literature references
3.19 »Quit--a structure in which one or more fibers, or
maintained in the laboratory for comparison to asbestos
fiber buadbes that are touching, arm attached to, or partially
concealed by a tingle particle or connected group of non-
asbestos
as
misidentified
not
are
they
that
so
minerals
fibrous particles. The exposed must meat the 65ber
minerals.
ter
al
definition (see 3.2.4,
Antlgoike.
6.1.1
Patygausfdte (An te).
6.1.2
3.2.10 structues—a term that is used to categorize all the
types of asbestos pattidcs which arc recorded during the
Halloys
6.1.3
analysis (such as fibers, bundler, dusters, and masrlce 4
PymW suns .
6.1.4
Final results of the test are always expressed In asbestos
Sepiaolits.
6.1.5
set
✓amlatlite
1
6.1.6
struettaus per square centimetre 6.1.7
Fibrous tak
those
than
other
Hornblende and other ampbt'boles
6.1.8
. 4. Summary of Test Method
in
listed 3.1.2.
aces
6.2
rticles in
mm
1
grosser:
pa
dust
any
Collecting than
4.1 The sample is collected by vacuuming a known in this test method may cause an
in ri
ce and. therefore,
surface area with a standard 25 or 37 mm air
sampling must be avoided.
cassette using a plastic tube that is attachnd to the inlet
orifice which acts as a nozzle The sample is transferred from 7. Materials and
Equipment
.
inside the casoe to an aqueous solution of known volume. 7.1 Pwby
g('Reagests-Reagent grade duals shalt
be
Aliquors of the suspension are then filtered through a used in all teens. Unless
athelrwige indicated, is is handed
membrane. A section of the membrane is prepared and that all reagents
conform to
the mo ons of the Com-
transferred to a TEM grid using the direct hen method. er
mittee
an Analytical Reaps of the American
Cbermical
b. The asbestiform structures are identified, sized, and counted Society, where such sp eciflenicus
are available. Other
grades
by ?EM, using SAED and EDXA at a ma r cation of may be us ed.
provided it is fist
ascertained that
the relent
I5 t10) to 20 OOOX. is
of sufficiently
high
purity to permit its use without
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