NYC 9/11 Public Portal Document
FEB-14-02 11:09 FROM-PACE ANALYTICAL 612-607-6444 T-452 P.03/04 F-677
1700 Elm Street - Suite 2GC
Minneapolis, MN 55414
nM
1 aceAnal "cal od 23 Analysis Results
Tel: 612-6D7-170C
Client - ATC
Client's Sample ID P-3 DUANE ST
Lab Sample 10 103286969
Filename F20212B_07 Matrix PUF
Injected By BAL Dilution NA
Amount Extracted 491.07 m3 Collected 01/23/2002
ICAL Date 01/25/2002 Received 01/25/2002
CCal Filename(s) F20212B_02 Extracted 01/29/2002
Method Blank ID BLANK-1441 Analyzed 02/13/2002 01:23
Native Conc EMPC LRL Internal ng's Percent
Isomers pg/m3 pg/m3 pg/m3 Standards Added Recovery
2,3,7,8-TCDF ---- 0.0270 0.0064 IA 2,3,7,8-TCDF-1 SC 2.00 69
Total TCDF 0.770 ----- 0.0041 2,3,7,8-TCDD-13C 2.00 72
1 ---- 1,2,3,7,8-PeCDF-13C 2.00 77
2,3,7,8-TCDD - 0.0055 0.0045 IA 1,2,3,7,8-PeCDD-13C 2.00 83
Total TCDD 2.000 --- 0.0041 1,2,3,6,7,8-HxCDF-13C 2.00 67
1,2,3,6,7,8-HxCDD-13C 2.00 67
1,2,3,7,8-PeCDF ----- 0.0310 0.0200 E 1,2,3,4,6,7,8-HpCDF-13C 2.00 62
2,3,4,7,8-PeCDF ND 0.0200 1,2,3,4,6,7,8-HpCDD-13C 2.00 68
Total PeCDF 0.320 ---- 0.0200 OCDD-13C 4.00 60
i,2,3,7.8-PeCDD ND 0.0200 Recovery
I Total PeCDO
1,2,3,4,7,8-HxCDF
0.370
----- 0.0330
0.0200
0.0200 E
Standards
1,2,3,4-TODD-13C
1,2,3,7,8.9-HxCDD-13C
2.00
2.00
NA
NA
1,2,3,6,7,8-HxCDF --- 0.0220 0.0200 E
2,3,4,6,7,8-HxCDF 0.026 0.0200 J Surrogates
1,2,3,7,8,9-HxCDF ND 0.0200 2,3,7,8-TCDD-37Cl4 2.00 103
Total HxCDF 0.150 ----- 0,0200 2,3,4,7,8-PeCDF-13C 2.00 103
----- 1,2,3,4,7,8-HxCDF-13C 2.00 118
I 1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
ND
ND
ND ---
0.0200
0.0200
0.0200
1,2,3,4,7,8-HxCDD-13C
1,2,3,4,7,8,9-HpCDF-13C
2.00
2.00
127
100
Total HxCDD 0.350 - 0.0200
•
1,2,3,4,6,7,8-HpCDF 0.048 0.0200 J Total 2,3,7,8-TCDD
1,2,3,4,7,8,9-HpCDF ND --- 0.0200 Equivalence: 0.0048 pg/m3
Total HpCDF 0.048 - 0.0200 J (Using ITE Factors)
L 1,2,3,4,6,7,8-HpCDD
Total HpCDD
0.110
0.200 -----
0.0200
0.0200
I OCDF
OCDD
0.056
0.590
:Y:_ 0.0410 J
0.0410
Conc = Concentration (Totals include 2,3,7,8-substituted isomers). I = Interference
EMPC = Estimated Maximum Possible Concentration E = PCDE Interference
LRL = Lower Reporting Limit S = Saturated signal
J = Concentration detected is below the calibration range NO = Not Detected
B = Less than 10 times higher than method thank level NA = Not Applicable
•
P = Recovery outside of target range NC = Not Calculated
Nn = Value obtained from additional analysis
A = Detection Limit based on signal to noise
Report No.....02-1053453
I
REPORT OF LABORATORY ANALYSIS
This report snail not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
NYC-WTC 000104551
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