Chlorinated pesticides analysis results, Nov-Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Signal #1 : C:\HPCHEM\1\DATA\5O8F\O1113OD\2PESTC2.D\ECD1A.CH Vial: 78 Signal #2 : C:\HPCHEM\l\DATA\508F\011130D\2PESTC2.D\ECD2B.CH Acq On : 2 Dec 2001 3:55 am Operator: Nefliu Sample : pest ccvl Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 11 8:27 2001 Quant Results File: 011204P.RES Quant Method : C:\HPCHEM\1\METHODS\508\011204P.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES 9/6/00 Last Update : Sun Oct 21 15:26:52 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/L ug/L

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 36.60 33.62 998363 1033859 0.209m 0.197m Spiked Amount 0.200 Recovery = 104.50% 98.50% Target Compounds 1) PROPACHLOR 16.36 15.23 198359 202641 0.238V‘’ 0.215m 2) g-BHC 22.45 20.11 2855652 3637498 0.327 I>VI- 0.297 lohl . 3) HEPTACHLOR 25.10 21.49 638532 954615 0.110 0.096 4) ALDRIN 27.78 23.53 1375744 1523781 0.133 ,1, 0.123 5) HEPTACHLOR EPOXI 31.77 28.81 2316537 2608856 0.273m 0.241 I flo;/ - 6) 4,4'-DDE 35.25 31.98 3694209 3887171 0.478m 0.378 7) DIELDRIN 35.52 32.64 696140 815495 0.095m„e'^ 0.076 8) ENDRIN 37.50 33.69 1110996 1536622 0.341’m 0.208m# 9) METHOXYCHLOR 48.37 40.58 758060 987899 0-514 0.324m# /i/.

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(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 011204P.M Tue Dec 11 08:29:52 2001 Page 1

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