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Document / 9 pages

DEP pesticide analysis results, AD27013, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting pesticide and PCB analysis for sample AD27013 from November to December 2001.

NYC-WTC_000091003–000091011

Folder label: “508 X 11/9/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011207\27013.D\ECDlA.CH Vial: 36 Signal #2 : C:\MSDCHEM\l\DATA\508\011207\27013.D\ECD2B.CH Acq On : 08 Dec 2001 7:03 am Operator: Nefliu Sample : sample Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 18 16:04:52 2001 Quant Results File: 011208P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011208P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 17 10:38:25 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.46 15.05 526.3E6 419.6E6 0.161m 0.178 Spiked Amount 0.200 Recovery 80.50% 89.00%

Target Compounds 1) Propachlor 9.14 8.57 2461427 2624884 0.005m 0.008m# 3) Heptachlor 11.11 11.32 5668345 3895882 0.001m 0.001m 4) Aldrin 11.79 12.06 1505599 11173202 0.000m 0.002 # 5) Heptachlor Epoxi 13.25 13.38 4340344 63264377 0.001m 0.013 # 6) 4,4-DDE 14.08 14.61 35906738 26989064 0.006m 0.006 7) Dieldrin 14.67 14.88 4038831 4134427 0.001m 0.001m# 8) Endrin 15.17 15.54 2164131 3380134 0.001m 0.001m# 9) Methoxychlor 17.11 18.08 12103348 77173752 0.006m 0.069 #

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 27013.D 011208P.M Tue Dec 18 16:07:41 2001 Page 1

NYC-WTC_000091004

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NYC-WTC_000091004Source: NYC Law Department, mirrored locally

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