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Pesticide analysis results below detection limits for sample AD28309

Machine-extracted title · confidence 100%

Laboratory report indicating pesticide concentrations were below method detection limits for sample AD28309 collected in late 2001.

NYC-WTC_000056875–000056883

Folder label: “508 X 11/26/01 A 12/21 - 12/22/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011221B\28309.D\ECDlA.CH Vial: 44 Signal #2 : C:\MSDCHEM\l\DATA\508\011221B\28309.D\ECD2B.CH Acq On : 22 Dec 2001 8:56 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 09 11:13:04 2002 Quant Results File: 011220P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011220P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Dec 21 08:18:43 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 625.3E6 469.3E6 0.169 0.168 Spiked Amount 0.200 Recovery 84.50% 84.00%

Target Compounds 1) Propachlor 9.04 8.48 10199242 3899109 0.021 0.011m# 2) g-BHC 9.85 10.26 6208003 8020771 0.001 0.001 # 3) Heptachlor 11.00 11.25 3335918 5464332 0.000 0.001 # 4) Aldrin 11.69 12.00 7786767 9930267 0.001 0.002 # 5) Heptachlor Epoxi 13.16 13.57 7599598 12341956 0.001 0.002 # 6) 4,4-DDE 13.98 14.75 7742862 4872456 0.001 0.001 7) Dieldrin 14.55 14.75 6934159 4872456 0.001 0.001 8) Endrin 15.04 15.81f 9629672 3953054 0,002 0.001 # 9) Methoxychlor 0.00 18.01 0 11440783 N.D. d 0.009

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 28309.D 011220P.M Wed Jan 09 11:13:56 2002 Page 1

NYC-WTC_000056876

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NYC-WTC_000056876Source: NYC Law Department, mirrored locally

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