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DEP Lab Results: Pesticide CCV2 Analysis, Sample AD31072

Machine-extracted title · confidence 90%

Second calibration verification data for pesticide analysis of sample AD31072 showing recovery percentages in January 2002.

NYC-WTC_000090540–000090543

Folder label: “508 X 12/21/01 A 1/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\1221REFP.D\ECDlA.CHVial: 23 Signal #2 -. C:\MSDCHEM\l\DATA\508\020103C\1221REFP.D\ECD2B.CH Acq On : 04 Jan 2002 1:06 am Operator: Nefliu Sample : 12/21 ref pest Inst Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 11:02:06 2002 Quant Results File: 020103P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020103P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Jan 04 10:51:09 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 14.36 14.97 778.7E6 672.7E6 0.210 0.216 Spilled Amount 0.2 00 Recovery = 105.00% 108.00%

Target Compounds 1) Propachlor 9.06 8.49 137.5E6 113.5E6 0.265 0.284 2) g'-BHC 9.83 10.18 1806.8E6 1480.4E6 0.223 0.230 3) Heptachlor 11.00 11.23 802.2E6 580.6E6 0.107 0.110 4) Aldrin 11.71 11.98 333.9E6 272.5E6 0.041 0.042 5) Heptachlor Epoxi 13.15 13.33 1623.1E6 1318.7E6 0.227 0.234 6) 4,4-DDE 13.98 14.54 3694.6E6 3018.8E6 0.578 0.593 7) Dieldrin 14.57 14.80 892.3E6 763.6E6 0.121m 0.121 8) Endrin 15.07 15.46 828.8E6 674.5E6 0.165 0.172 9) Methoxychlor 17.02 18.01 748.8E6 520.5E6 0.340 0.352

(f)=RT Delta 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1221REFP.D 020103P.M Fri Jan 04 11:02:30 2002 Page 1

NYC-WTC_000090542

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NYC-WTC_000090542Source: NYC Law Department, mirrored locally

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