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DEP Lab Results: Pesticide CCV2 Analysis, Sample AD31072

Machine-extracted title · confidence 90%

Calibration verification data for pesticide analysis of sample AD31072 showing recovery percentages in January 2002.

NYC-WTC_000090533–000090539

Folder label: “508 X 12/21/01 A 1/3/02

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Scanned page image, NYC-WTC_000090534
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\2PESTC2.D\ECDlA.CHVial: 57 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\2PESTC2.D\ECD2B.CH Acq On : 04 Jan 2002 5:26 pm Operator Nefliu Sample : pest cev Inst Instrumen Mise : Multiplr 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 07 08:49:25 2002 Quant Results File: 020103P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020103P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Jan 04 10:51:09 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 14.36 14.97 680.1E6 609.9E6 0.183 0.196 Spilled Amount 0.200 Recovery 91.50% 98.00%

Target Compounds 1) Propachlor 9.06 8.49 88387993 73641692 0.170 8^ 0.184 2) g-BHC 9.83 10.18 2138.8E6 1822.9E6 0.264-34 0.283 3) Heptachlor 11.00 11.23 654.0E6 505.0E6 0.087^^/ 0.096 4) Aldrin 11.71 11.98 901.8E6 772.8E6 0.111*1 0.120 5) Heptachlor Epoxi 13.15 13.33 1595.0E6 1336.7E6 0.223<3 0.237 6) 4,4-DDE 13.98 14.54 2436.4E6 2066.2E6 O.SSl'jT 0.406 7) Dieldrin 14.57 14.80 544.6E6 489.9E6 0.074m 0.077 8) Endrin 15.07 15.46 933.1E6 798.2E6 0.186 *13 0.203 9) Methoxychlor 17.02 18.01 819.6E6 592.4E6 0.373 0.400

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 020103C.M Mon Jan 07 10:56:10 2002 Page 1

NYC-WTC_000090534

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NYC-WTC_000090534Source: NYC Law Department, mirrored locally

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