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← Document results/DEP Box 68/508 X 12/21/01 A 1/3/02
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DEP Lab Results: Pesticide CCV2 Analysis, Sample AD31072

Machine-extracted title · confidence 90%

Calibration verification data for pesticide analysis of sample AD31072 showing recovery percentages in January 2002.

NYC-WTC_000090533–000090539

Folder label: “508 X 12/21/01 A 1/3/02

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Scanned page image, NYC-WTC_000090536
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\2CHLC3.D\ECDlA.CHVial: 55 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\2CHLC3.D\ECD2B.CH Acq On : 04 Jan 2002 4:28 pm Operator: Nefliu Sample : chl cev Inst Instrumen Mise : ■ Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 07 10:40:54 2002 Quant Results File: 020103C.RES

Quant Method : C:\MSDCHEM\1\METHODS\020103C.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Chlordane Last Update : Fri Jan 04 11:27:42 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 4) s 2,4-DDD SURROGAT 14.36 14.97 556.7E6 528.6E6 0.166m 0.196m Spiked Amount 0.200 Recovery 83.00% 98.00%

Target Compounds 1) Chlordane Peak 1 10.81 10.88 341.3E6 298.3E6 1.354m 1.530 2) Chlordane Peak 2 12.07 12.39 396.0E6 310.3E6 1.338m 1.499m 3) Chlordane Peak 3 13.44 13.76 1199.1E6 946.7E6 1.395m 1.583m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2CHLC3.D 020103C.M Mon Jan 07 10:56:01 2002 Page 1

NYC-WTC_000090536

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NYC-WTC_000090536Source: NYC Law Department, mirrored locally

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