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← Document results/DEP Box 68/508 X 12/21/01 A 1/3/02
Document / 9 pages

Pesticide calibration verification results, sample AD31072, Jan 2002

Machine-extracted title · confidence 95%

Calibration data showing recovery percentages for various pesticide standards in sample AD31072.

NYC-WTC_000090524–000090532

Folder label: “508 X 12/21/01 A 1/3/02

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Scanned page image, NYC-WTC_000090527
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O2O1O3C\CHLC1.D\ECD1A.CH Vial: 6 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\CHLCl.D\ECD2B.CH Acq On : 03 Jan 2002 4:56 pm Operator: Nefliu Sample : chl id Inst Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 11:28:02 2002 Quant Results File: 020103C.RES

Quant Method : C:\MSDCHEM\1\METHODS\020103C.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Chlordane Last Update : Fri Jan 04 11:27:42 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 4) s 2,4-DDD SURROGAT 14.36 14.98 755.4E6 544.1E6 0.225m 0.202 Spiked Amount 0.200 Recovery = 112.50% 101.00%

Target Compounds 1) Chlordane Peak 1 10.81 10.88 102.2E6 76362259 0.406m 0.392 2) Chlordane Peak 2 12.08 12.39 128.0E6 91038762 0.433m 0.440m 3) Chlordane Peak 3 13.44 13.76 347.3E6 235.0E6 0.404m 0.394m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. CHLCl.D 020103C.M Mon Jan 07 10:56:28 2002 Page 1

NYC-WTC_000090527

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NYC-WTC_000090527Source: NYC Law Department, mirrored locally

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